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Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS
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Zeitschriftentitel: | Journal of AOAC INTERNATIONAL |
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Personen und Körperschaften: | , , , , , , , |
In: | Journal of AOAC INTERNATIONAL, 103, 2020, 3, S. 699-704 |
Format: | E-Article |
Sprache: | Englisch |
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Oxford University Press (OUP)
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Schlagwörter: |
author_facet |
Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed |
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author |
Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed |
spellingShingle |
Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed Journal of AOAC INTERNATIONAL Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry |
author_sort |
zahiruddin, sultan |
spelling |
Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed 1060-3271 1944-7922 Oxford University Press (OUP) Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry http://dx.doi.org/10.5740/jaoacint.19-0230 <jats:title>Abstract</jats:title> <jats:p>Background: There is an increasing global demand for traditional medicines because of their efficacy, ease of availability, and few or no side effects. The Unani medicines have long been used in India and abroad for various disorders and diseases. Arqiyat (Arq; distillate) is one of the most widely used Unani formulation prepared by simple distillation from single or combination drugs. Objective: In the present investigation, an attempt has been made to generate data for quality control and stability testing of Arq formulations of the Unani Pharmacopeia of India that includes only three Arq formulations. Method: Arq-e-Nana (AeN), Arq-e-Gazar (AeG), and Arq-e-Brinjasif (AeB) were prepared through hydrodistillation. Quality control and stability analysis were performed by using HPTLC and GC-MS. Results: Dichloromethane extract of AeB showed maximum of 10 bands at different retardation factor values; however, there are 7 bands in AeN as well as in AeG. GC-MS analysis showed presence of 10 metabolites in AeG, 8 in AeN, and 9 in AeB. Stability studies showed that the shelf life of Arq formulations would be enhanced at refrigeration (5 ± 2°C) conditions. Conclusions: The present study highlights quality control and stability analysis of Arq formulations of Unani Pharmacopeia of India using HPTLC and GC-MS.</jats:p> Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS Journal of AOAC INTERNATIONAL |
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10.5740/jaoacint.19-0230 |
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Online |
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Chemie und Pharmazie Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft Technik |
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2020 |
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Journal of AOAC INTERNATIONAL |
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title |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_unstemmed |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_full |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_fullStr |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_full_unstemmed |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_short |
Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_sort |
quality control and stability testing of arq formulations of unani pharmacopeia of india using hptlc and gc-ms |
topic |
Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry |
url |
http://dx.doi.org/10.5740/jaoacint.19-0230 |
publishDate |
2020 |
physical |
699-704 |
description |
<jats:title>Abstract</jats:title>
<jats:p>Background: There is an increasing global demand for traditional medicines because of their efficacy, ease of availability, and few or no side effects. The Unani medicines have long been used in India and abroad for various disorders and diseases. Arqiyat (Arq; distillate) is one of the most widely used Unani formulation prepared by simple distillation from single or combination drugs. Objective: In the present investigation, an attempt has been made to generate data for quality control and stability testing of Arq formulations of the Unani Pharmacopeia of India that includes only three Arq formulations. Method: Arq-e-Nana (AeN), Arq-e-Gazar (AeG), and Arq-e-Brinjasif (AeB) were prepared through hydrodistillation. Quality control and stability analysis were performed by using HPTLC and GC-MS. Results: Dichloromethane extract of AeB showed maximum of 10 bands at different retardation factor values; however, there are 7 bands in AeN as well as in AeG. GC-MS analysis showed presence of 10 metabolites in AeG, 8 in AeN, and 9 in AeB. Stability studies showed that the shelf life of Arq formulations would be enhanced at refrigeration (5 ± 2°C) conditions. Conclusions: The present study highlights quality control and stability analysis of Arq formulations of Unani Pharmacopeia of India using HPTLC and GC-MS.</jats:p> |
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author | Zahiruddin, Sultan, Parveen, Abida, Khan, Washim, Ibrahim, Mohammad, Akhtar, Jamal, Khan, Asim Ali, Ansari, S H, Ahmad, Sayeed |
author_facet | Zahiruddin, Sultan, Parveen, Abida, Khan, Washim, Ibrahim, Mohammad, Akhtar, Jamal, Khan, Asim Ali, Ansari, S H, Ahmad, Sayeed, Zahiruddin, Sultan, Parveen, Abida, Khan, Washim, Ibrahim, Mohammad, Akhtar, Jamal, Khan, Asim Ali, Ansari, S H, Ahmad, Sayeed |
author_sort | zahiruddin, sultan |
container_issue | 3 |
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container_title | Journal of AOAC INTERNATIONAL |
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description | <jats:title>Abstract</jats:title> <jats:p>Background: There is an increasing global demand for traditional medicines because of their efficacy, ease of availability, and few or no side effects. The Unani medicines have long been used in India and abroad for various disorders and diseases. Arqiyat (Arq; distillate) is one of the most widely used Unani formulation prepared by simple distillation from single or combination drugs. Objective: In the present investigation, an attempt has been made to generate data for quality control and stability testing of Arq formulations of the Unani Pharmacopeia of India that includes only three Arq formulations. Method: Arq-e-Nana (AeN), Arq-e-Gazar (AeG), and Arq-e-Brinjasif (AeB) were prepared through hydrodistillation. Quality control and stability analysis were performed by using HPTLC and GC-MS. Results: Dichloromethane extract of AeB showed maximum of 10 bands at different retardation factor values; however, there are 7 bands in AeN as well as in AeG. GC-MS analysis showed presence of 10 metabolites in AeG, 8 in AeN, and 9 in AeB. Stability studies showed that the shelf life of Arq formulations would be enhanced at refrigeration (5 ± 2°C) conditions. Conclusions: The present study highlights quality control and stability analysis of Arq formulations of Unani Pharmacopeia of India using HPTLC and GC-MS.</jats:p> |
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spelling | Zahiruddin, Sultan Parveen, Abida Khan, Washim Ibrahim, Mohammad Akhtar, Jamal Khan, Asim Ali Ansari, S H Ahmad, Sayeed 1060-3271 1944-7922 Oxford University Press (OUP) Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry http://dx.doi.org/10.5740/jaoacint.19-0230 <jats:title>Abstract</jats:title> <jats:p>Background: There is an increasing global demand for traditional medicines because of their efficacy, ease of availability, and few or no side effects. The Unani medicines have long been used in India and abroad for various disorders and diseases. Arqiyat (Arq; distillate) is one of the most widely used Unani formulation prepared by simple distillation from single or combination drugs. Objective: In the present investigation, an attempt has been made to generate data for quality control and stability testing of Arq formulations of the Unani Pharmacopeia of India that includes only three Arq formulations. Method: Arq-e-Nana (AeN), Arq-e-Gazar (AeG), and Arq-e-Brinjasif (AeB) were prepared through hydrodistillation. Quality control and stability analysis were performed by using HPTLC and GC-MS. Results: Dichloromethane extract of AeB showed maximum of 10 bands at different retardation factor values; however, there are 7 bands in AeN as well as in AeG. GC-MS analysis showed presence of 10 metabolites in AeG, 8 in AeN, and 9 in AeB. Stability studies showed that the shelf life of Arq formulations would be enhanced at refrigeration (5 ± 2°C) conditions. Conclusions: The present study highlights quality control and stability analysis of Arq formulations of Unani Pharmacopeia of India using HPTLC and GC-MS.</jats:p> Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS Journal of AOAC INTERNATIONAL |
spellingShingle | Zahiruddin, Sultan, Parveen, Abida, Khan, Washim, Ibrahim, Mohammad, Akhtar, Jamal, Khan, Asim Ali, Ansari, S H, Ahmad, Sayeed, Journal of AOAC INTERNATIONAL, Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS, Pharmacology, Agronomy and Crop Science, Environmental Chemistry, Food Science, Analytical Chemistry |
title | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_full | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_fullStr | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_full_unstemmed | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_short | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
title_sort | quality control and stability testing of arq formulations of unani pharmacopeia of india using hptlc and gc-ms |
title_unstemmed | Quality Control and Stability Testing of Arq Formulations of Unani Pharmacopeia of India Using HPTLC and GC-MS |
topic | Pharmacology, Agronomy and Crop Science, Environmental Chemistry, Food Science, Analytical Chemistry |
url | http://dx.doi.org/10.5740/jaoacint.19-0230 |