author_facet Kuwano, Noriyuki
Horikami, Sadanori
Linus, Marina
Kuwano, Noriyuki
Horikami, Sadanori
Linus, Marina
author Kuwano, Noriyuki
Horikami, Sadanori
Linus, Marina
spellingShingle Kuwano, Noriyuki
Horikami, Sadanori
Linus, Marina
Materials Science Forum
Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
Mechanical Engineering
Mechanics of Materials
Condensed Matter Physics
General Materials Science
author_sort kuwano, noriyuki
spelling Kuwano, Noriyuki Horikami, Sadanori Linus, Marina 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.827.341 <jats:p>The changes of microstructure in pure-Sn after deformation were investigated by electron microscopy. Two types of specimens were prepared: Sample-1; pure-Sn/Fe-42Ni, Sample-2; single crystalline pure-Sn. The growth of curling whiskers on Sample-1 was observed <jats:italic>in-situ</jats:italic> in a scanning electron microscope (SEM). A thin foil specimen of the curling whisker was made with a focused ion beam (FIB) mill. Transmission electron microscope (TEM) analysis confirmed that the curling whisker was of a single crystal regardless of its external shape. New models for growth process of a bent single-crystalline whisker were proposed. The models are composed of epitaxial growth and recrystallization. Electron back scatter diffraction (EBSD) analysis was performed for Sample-2. The results of EBSD strongly suggested that recrystallization proceeds even at room temperature. These experimental results are very important to understand the behavior of dynamical deformation and recrystallization of Sn metal, and useful in consideration the mitigation of whiskers.</jats:p> Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers Materials Science Forum
doi_str_mv 10.4028/www.scientific.net/msf.827.341
facet_avail Online
finc_class_facet Physik
Technik
format ElectronicArticle
fullrecord blob:ai-49-aHR0cDovL2R4LmRvaS5vcmcvMTAuNDAyOC93d3cuc2NpZW50aWZpYy5uZXQvbXNmLjgyNy4zNDE
id ai-49-aHR0cDovL2R4LmRvaS5vcmcvMTAuNDAyOC93d3cuc2NpZW50aWZpYy5uZXQvbXNmLjgyNy4zNDE
institution DE-Pl11
DE-Rs1
DE-105
DE-14
DE-Ch1
DE-L229
DE-D275
DE-Bn3
DE-Brt1
DE-D161
DE-Gla1
DE-Zi4
DE-15
imprint Trans Tech Publications, Ltd., 2015
imprint_str_mv Trans Tech Publications, Ltd., 2015
issn 1662-9752
issn_str_mv 1662-9752
language Undetermined
mega_collection Trans Tech Publications, Ltd. (CrossRef)
match_str kuwano2015electronmicroscopystudyofgrainboundarybehaviorinpbfreesoldermaterialsformitigationofwhiskers
publishDateSort 2015
publisher Trans Tech Publications, Ltd.
recordtype ai
record_format ai
series Materials Science Forum
source_id 49
title Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_unstemmed Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_full Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_fullStr Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_full_unstemmed Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_short Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_sort electron microscopy study of grain boundary behavior in pb-free solder materials for mitigation of whiskers
topic Mechanical Engineering
Mechanics of Materials
Condensed Matter Physics
General Materials Science
url http://dx.doi.org/10.4028/www.scientific.net/msf.827.341
publishDate 2015
physical 341-346
description <jats:p>The changes of microstructure in pure-Sn after deformation were investigated by electron microscopy. Two types of specimens were prepared: Sample-1; pure-Sn/Fe-42Ni, Sample-2; single crystalline pure-Sn. The growth of curling whiskers on Sample-1 was observed <jats:italic>in-situ</jats:italic> in a scanning electron microscope (SEM). A thin foil specimen of the curling whisker was made with a focused ion beam (FIB) mill. Transmission electron microscope (TEM) analysis confirmed that the curling whisker was of a single crystal regardless of its external shape. New models for growth process of a bent single-crystalline whisker were proposed. The models are composed of epitaxial growth and recrystallization. Electron back scatter diffraction (EBSD) analysis was performed for Sample-2. The results of EBSD strongly suggested that recrystallization proceeds even at room temperature. These experimental results are very important to understand the behavior of dynamical deformation and recrystallization of Sn metal, and useful in consideration the mitigation of whiskers.</jats:p>
container_start_page 341
container_title Materials Science Forum
container_volume 827
format_de105 Article, E-Article
format_de14 Article, E-Article
format_de15 Article, E-Article
format_de520 Article, E-Article
format_de540 Article, E-Article
format_dech1 Article, E-Article
format_ded117 Article, E-Article
format_degla1 E-Article
format_del152 Buch
format_del189 Article, E-Article
format_dezi4 Article
format_dezwi2 Article, E-Article
format_finc Article, E-Article
format_nrw Article, E-Article
_version_ 1792321194496622592
geogr_code not assigned
last_indexed 2024-03-01T10:58:09.39Z
geogr_code_person not assigned
openURL url_ver=Z39.88-2004&ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fvufind.svn.sourceforge.net%3Agenerator&rft.title=Electron+Microscopy+Study+of+Grain+Boundary+Behavior+in+Pb-Free+Solder+Materials+for+Mitigation+of+Whiskers&rft.date=2015-08-01&genre=article&issn=1662-9752&volume=827&spage=341&epage=346&pages=341-346&jtitle=Materials+Science+Forum&atitle=Electron+Microscopy+Study+of+Grain+Boundary+Behavior+in+Pb-Free+Solder+Materials+for+Mitigation+of+Whiskers&aulast=Linus&aufirst=Marina&rft_id=info%3Adoi%2F10.4028%2Fwww.scientific.net%2Fmsf.827.341&rft.language%5B0%5D=und
SOLR
_version_ 1792321194496622592
author Kuwano, Noriyuki, Horikami, Sadanori, Linus, Marina
author_facet Kuwano, Noriyuki, Horikami, Sadanori, Linus, Marina, Kuwano, Noriyuki, Horikami, Sadanori, Linus, Marina
author_sort kuwano, noriyuki
container_start_page 341
container_title Materials Science Forum
container_volume 827
description <jats:p>The changes of microstructure in pure-Sn after deformation were investigated by electron microscopy. Two types of specimens were prepared: Sample-1; pure-Sn/Fe-42Ni, Sample-2; single crystalline pure-Sn. The growth of curling whiskers on Sample-1 was observed <jats:italic>in-situ</jats:italic> in a scanning electron microscope (SEM). A thin foil specimen of the curling whisker was made with a focused ion beam (FIB) mill. Transmission electron microscope (TEM) analysis confirmed that the curling whisker was of a single crystal regardless of its external shape. New models for growth process of a bent single-crystalline whisker were proposed. The models are composed of epitaxial growth and recrystallization. Electron back scatter diffraction (EBSD) analysis was performed for Sample-2. The results of EBSD strongly suggested that recrystallization proceeds even at room temperature. These experimental results are very important to understand the behavior of dynamical deformation and recrystallization of Sn metal, and useful in consideration the mitigation of whiskers.</jats:p>
doi_str_mv 10.4028/www.scientific.net/msf.827.341
facet_avail Online
finc_class_facet Physik, Technik
format ElectronicArticle
format_de105 Article, E-Article
format_de14 Article, E-Article
format_de15 Article, E-Article
format_de520 Article, E-Article
format_de540 Article, E-Article
format_dech1 Article, E-Article
format_ded117 Article, E-Article
format_degla1 E-Article
format_del152 Buch
format_del189 Article, E-Article
format_dezi4 Article
format_dezwi2 Article, E-Article
format_finc Article, E-Article
format_nrw Article, E-Article
geogr_code not assigned
geogr_code_person not assigned
id ai-49-aHR0cDovL2R4LmRvaS5vcmcvMTAuNDAyOC93d3cuc2NpZW50aWZpYy5uZXQvbXNmLjgyNy4zNDE
imprint Trans Tech Publications, Ltd., 2015
imprint_str_mv Trans Tech Publications, Ltd., 2015
institution DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229, DE-D275, DE-Bn3, DE-Brt1, DE-D161, DE-Gla1, DE-Zi4, DE-15
issn 1662-9752
issn_str_mv 1662-9752
language Undetermined
last_indexed 2024-03-01T10:58:09.39Z
match_str kuwano2015electronmicroscopystudyofgrainboundarybehaviorinpbfreesoldermaterialsformitigationofwhiskers
mega_collection Trans Tech Publications, Ltd. (CrossRef)
physical 341-346
publishDate 2015
publishDateSort 2015
publisher Trans Tech Publications, Ltd.
record_format ai
recordtype ai
series Materials Science Forum
source_id 49
spelling Kuwano, Noriyuki Horikami, Sadanori Linus, Marina 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.827.341 <jats:p>The changes of microstructure in pure-Sn after deformation were investigated by electron microscopy. Two types of specimens were prepared: Sample-1; pure-Sn/Fe-42Ni, Sample-2; single crystalline pure-Sn. The growth of curling whiskers on Sample-1 was observed <jats:italic>in-situ</jats:italic> in a scanning electron microscope (SEM). A thin foil specimen of the curling whisker was made with a focused ion beam (FIB) mill. Transmission electron microscope (TEM) analysis confirmed that the curling whisker was of a single crystal regardless of its external shape. New models for growth process of a bent single-crystalline whisker were proposed. The models are composed of epitaxial growth and recrystallization. Electron back scatter diffraction (EBSD) analysis was performed for Sample-2. The results of EBSD strongly suggested that recrystallization proceeds even at room temperature. These experimental results are very important to understand the behavior of dynamical deformation and recrystallization of Sn metal, and useful in consideration the mitigation of whiskers.</jats:p> Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers Materials Science Forum
spellingShingle Kuwano, Noriyuki, Horikami, Sadanori, Linus, Marina, Materials Science Forum, Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers, Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science
title Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_full Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_fullStr Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_full_unstemmed Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_short Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
title_sort electron microscopy study of grain boundary behavior in pb-free solder materials for mitigation of whiskers
title_unstemmed Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of Whiskers
topic Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science
url http://dx.doi.org/10.4028/www.scientific.net/msf.827.341