author_facet Saida, Kazuyoshi
Ogiwara, Hiroyuki
Nishimoto, Kazutoshi
Saida, Kazuyoshi
Ogiwara, Hiroyuki
Nishimoto, Kazutoshi
author Saida, Kazuyoshi
Ogiwara, Hiroyuki
Nishimoto, Kazutoshi
spellingShingle Saida, Kazuyoshi
Ogiwara, Hiroyuki
Nishimoto, Kazutoshi
Materials Science Forum
Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
Mechanical Engineering
Mechanics of Materials
Condensed Matter Physics
General Materials Science
author_sort saida, kazuyoshi
spelling Saida, Kazuyoshi Ogiwara, Hiroyuki Nishimoto, Kazutoshi 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.706-709.3010 <jats:p>A new bonding technique of titanium and zirconium conducted at low temperatures was developed utilizing the hydrogen-induced transformation. Hydrogen charge treatment of the faying surfaces of titanium and zirconium was conducted with varying the charging time between 3.6-700ks prior to diffusion bonding. Diffusion bonding of hydrogen-charged titanium and zirconium was carried out at 600-800°C for 0.6-1.8ks applying the bonding pressure of 5-10MPa in vacuum. Titanium and zirconium hydrides were formed at faying surfaces after hydrogen charge treatment. The β-transus temperature at faying surfaces of titanium and zirconium was reduced to approx. 450-550°C with hydrogen-charging. The bond layer was phase transformed to a bcc structure (β) at the bonding temperature due to the hydrogen diffusion during bonding process. Grain growth across the prior bond interface was observed in the joints bonded at 750-800°C after hydrogen-charging for 300-500ks. Tensile strength of titanium joints bonded at 800°C attained approx. 70% of the base metal strength (approx. 1.6 times as high as non-charged joints), and corrosion resistance of the joints was comparable to that of the base metal. Furthermore, tensile strength of zirconium joints bonded at 800°C was approx. 1.7 times as high as non-charged joints. It follows that the solid-state bondability of titanium and zirconium at low temperatures was improved compared to the conventional diffusion bonding (direct bonding without hydrogen-charging).</jats:p> Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation Materials Science Forum
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title Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_unstemmed Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_full Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_fullStr Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_full_unstemmed Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_short Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_sort development of low temperature bonding technique of titanium and zirconium using hydrogen diffusion-induced phase transformation
topic Mechanical Engineering
Mechanics of Materials
Condensed Matter Physics
General Materials Science
url http://dx.doi.org/10.4028/www.scientific.net/msf.706-709.3010
publishDate 2012
physical 3010-3015
description <jats:p>A new bonding technique of titanium and zirconium conducted at low temperatures was developed utilizing the hydrogen-induced transformation. Hydrogen charge treatment of the faying surfaces of titanium and zirconium was conducted with varying the charging time between 3.6-700ks prior to diffusion bonding. Diffusion bonding of hydrogen-charged titanium and zirconium was carried out at 600-800°C for 0.6-1.8ks applying the bonding pressure of 5-10MPa in vacuum. Titanium and zirconium hydrides were formed at faying surfaces after hydrogen charge treatment. The β-transus temperature at faying surfaces of titanium and zirconium was reduced to approx. 450-550°C with hydrogen-charging. The bond layer was phase transformed to a bcc structure (β) at the bonding temperature due to the hydrogen diffusion during bonding process. Grain growth across the prior bond interface was observed in the joints bonded at 750-800°C after hydrogen-charging for 300-500ks. Tensile strength of titanium joints bonded at 800°C attained approx. 70% of the base metal strength (approx. 1.6 times as high as non-charged joints), and corrosion resistance of the joints was comparable to that of the base metal. Furthermore, tensile strength of zirconium joints bonded at 800°C was approx. 1.7 times as high as non-charged joints. It follows that the solid-state bondability of titanium and zirconium at low temperatures was improved compared to the conventional diffusion bonding (direct bonding without hydrogen-charging).</jats:p>
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author Saida, Kazuyoshi, Ogiwara, Hiroyuki, Nishimoto, Kazutoshi
author_facet Saida, Kazuyoshi, Ogiwara, Hiroyuki, Nishimoto, Kazutoshi, Saida, Kazuyoshi, Ogiwara, Hiroyuki, Nishimoto, Kazutoshi
author_sort saida, kazuyoshi
container_start_page 3010
container_title Materials Science Forum
container_volume 706-709
description <jats:p>A new bonding technique of titanium and zirconium conducted at low temperatures was developed utilizing the hydrogen-induced transformation. Hydrogen charge treatment of the faying surfaces of titanium and zirconium was conducted with varying the charging time between 3.6-700ks prior to diffusion bonding. Diffusion bonding of hydrogen-charged titanium and zirconium was carried out at 600-800°C for 0.6-1.8ks applying the bonding pressure of 5-10MPa in vacuum. Titanium and zirconium hydrides were formed at faying surfaces after hydrogen charge treatment. The β-transus temperature at faying surfaces of titanium and zirconium was reduced to approx. 450-550°C with hydrogen-charging. The bond layer was phase transformed to a bcc structure (β) at the bonding temperature due to the hydrogen diffusion during bonding process. Grain growth across the prior bond interface was observed in the joints bonded at 750-800°C after hydrogen-charging for 300-500ks. Tensile strength of titanium joints bonded at 800°C attained approx. 70% of the base metal strength (approx. 1.6 times as high as non-charged joints), and corrosion resistance of the joints was comparable to that of the base metal. Furthermore, tensile strength of zirconium joints bonded at 800°C was approx. 1.7 times as high as non-charged joints. It follows that the solid-state bondability of titanium and zirconium at low temperatures was improved compared to the conventional diffusion bonding (direct bonding without hydrogen-charging).</jats:p>
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spelling Saida, Kazuyoshi Ogiwara, Hiroyuki Nishimoto, Kazutoshi 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.706-709.3010 <jats:p>A new bonding technique of titanium and zirconium conducted at low temperatures was developed utilizing the hydrogen-induced transformation. Hydrogen charge treatment of the faying surfaces of titanium and zirconium was conducted with varying the charging time between 3.6-700ks prior to diffusion bonding. Diffusion bonding of hydrogen-charged titanium and zirconium was carried out at 600-800°C for 0.6-1.8ks applying the bonding pressure of 5-10MPa in vacuum. Titanium and zirconium hydrides were formed at faying surfaces after hydrogen charge treatment. The β-transus temperature at faying surfaces of titanium and zirconium was reduced to approx. 450-550°C with hydrogen-charging. The bond layer was phase transformed to a bcc structure (β) at the bonding temperature due to the hydrogen diffusion during bonding process. Grain growth across the prior bond interface was observed in the joints bonded at 750-800°C after hydrogen-charging for 300-500ks. Tensile strength of titanium joints bonded at 800°C attained approx. 70% of the base metal strength (approx. 1.6 times as high as non-charged joints), and corrosion resistance of the joints was comparable to that of the base metal. Furthermore, tensile strength of zirconium joints bonded at 800°C was approx. 1.7 times as high as non-charged joints. It follows that the solid-state bondability of titanium and zirconium at low temperatures was improved compared to the conventional diffusion bonding (direct bonding without hydrogen-charging).</jats:p> Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation Materials Science Forum
spellingShingle Saida, Kazuyoshi, Ogiwara, Hiroyuki, Nishimoto, Kazutoshi, Materials Science Forum, Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation, Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science
title Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_full Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_fullStr Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_full_unstemmed Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_short Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
title_sort development of low temperature bonding technique of titanium and zirconium using hydrogen diffusion-induced phase transformation
title_unstemmed Development of Low Temperature Bonding Technique of Titanium and Zirconium Using Hydrogen Diffusion-Induced Phase Transformation
topic Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science
url http://dx.doi.org/10.4028/www.scientific.net/msf.706-709.3010