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Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization
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| Zeitschriftentitel: | Materials Science Forum |
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| Personen und Körperschaften: | , , , , , |
| In: | Materials Science Forum, 494, 2005, S. 333-338 |
| Format: | E-Article |
| Sprache: | Unbestimmt |
| veröffentlicht: |
Trans Tech Publications, Ltd.
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| Schlagwörter: |
| author_facet |
Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. |
|---|---|
| author |
Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. |
| spellingShingle |
Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. Materials Science Forum Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science |
| author_sort |
krstić, j. |
| spelling |
Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.494.333 <jats:p>The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)2×6H2O and Mg(NO3)2×6H2O of constant molar ratio, 2% solution of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90°C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110°C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N2 physisorption. The relation between synthesis procedure and precursor properties was established.</jats:p> Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization Materials Science Forum |
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| title |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_unstemmed |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_full |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_fullStr |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_full_unstemmed |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_short |
Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_sort |
nickel/silica precursor from sodium silicate solution - synthesis and characterization |
| topic |
Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science |
| url |
http://dx.doi.org/10.4028/www.scientific.net/msf.494.333 |
| publishDate |
2005 |
| physical |
333-338 |
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<jats:p>The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)2×6H2O and Mg(NO3)2×6H2O of constant molar ratio, 2% solution of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90°C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110°C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N2 physisorption. The relation between synthesis procedure and precursor properties was established.</jats:p> |
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| author | Krstić, J., Vukelić, N., Nedić, Zoran, Milutinović-Nikolić, A., Šućurović, A., Jovanović, D. |
| author_facet | Krstić, J., Vukelić, N., Nedić, Zoran, Milutinović-Nikolić, A., Šućurović, A., Jovanović, D., Krstić, J., Vukelić, N., Nedić, Zoran, Milutinović-Nikolić, A., Šućurović, A., Jovanović, D. |
| author_sort | krstić, j. |
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| container_title | Materials Science Forum |
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| description | <jats:p>The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)2×6H2O and Mg(NO3)2×6H2O of constant molar ratio, 2% solution of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90°C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110°C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N2 physisorption. The relation between synthesis procedure and precursor properties was established.</jats:p> |
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| physical | 333-338 |
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| spelling | Krstić, J. Vukelić, N. Nedić, Zoran Milutinović-Nikolić, A. Šućurović, A. Jovanović, D. 1662-9752 Trans Tech Publications, Ltd. Mechanical Engineering Mechanics of Materials Condensed Matter Physics General Materials Science http://dx.doi.org/10.4028/www.scientific.net/msf.494.333 <jats:p>The aim of this paper was the investigation of the influence of synthesis parameters, as well as the order of synthesis steps, in procedure of chemical precipitation, on the properties of synthesized nickel precursor. The starting materials were always the same aqueous solutions of Ni(NO3)2×6H2O and Mg(NO3)2×6H2O of constant molar ratio, 2% solution of SiO2 in the form of sodium silicate solution (module SiO2/Na2O = 3.0) and 10% solution of Na2CO3, while synthesis steps and addition modes were varied. Complete pH and temperature monitoring was performed during entire synthesis at 90°C. The formed precipitate aged 30 minutes at synthesis temperature. By changing the order and conditions of adding SiO2 and Na2CO3 solutions and keeping the treatment of precipitates the same (rinsing with hot distilled water followed by drying at 110°C for 24 hours) six different precursors were obtained. Samples characterizations were performed using different experimental techniques: XRD analysis, IR spectroscopy, reflection spectroscopy, TG analysis, N2 physisorption. The relation between synthesis procedure and precursor properties was established.</jats:p> Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization Materials Science Forum |
| spellingShingle | Krstić, J., Vukelić, N., Nedić, Zoran, Milutinović-Nikolić, A., Šućurović, A., Jovanović, D., Materials Science Forum, Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization, Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science |
| title | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_full | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_fullStr | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_full_unstemmed | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_short | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| title_sort | nickel/silica precursor from sodium silicate solution - synthesis and characterization |
| title_unstemmed | Nickel/Silica Precursor from Sodium Silicate Solution - Synthesis and Characterization |
| topic | Mechanical Engineering, Mechanics of Materials, Condensed Matter Physics, General Materials Science |
| url | http://dx.doi.org/10.4028/www.scientific.net/msf.494.333 |