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Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6...
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| Zeitschriftentitel: | Zeitschrift für Kristallographie - New Crystal Structures |
|---|---|
| Personen und Körperschaften: | , , |
| In: | Zeitschrift für Kristallographie - New Crystal Structures, 219, 2004, 2, S. 101-105 |
| Format: | E-Article |
| Sprache: | Unbestimmt |
| veröffentlicht: |
Walter de Gruyter GmbH
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| Schlagwörter: |
| author_facet |
Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich |
|---|---|
| author |
Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich |
| spellingShingle |
Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich Zeitschrift für Kristallographie - New Crystal Structures Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) Inorganic Chemistry Condensed Matter Physics General Materials Science |
| author_sort |
rabe, susanne |
| spelling |
Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich 2197-4578 1433-7266 Walter de Gruyter GmbH Inorganic Chemistry Condensed Matter Physics General Materials Science http://dx.doi.org/10.1524/ncrs.2004.219.2.101 <jats:title>Abstract</jats:title><jats:p> C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>4</jats:sub>N<jats:sub>4</jats:sub>OP<jats:sub>2</jats:sub>V, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.473(2) Å, <jats:italic>b </jats:italic>= 19.832(6) Å, <jats:italic>c </jats:italic>= 14.461(2) Å, β = 99.00(2)°, <jats:italic>V </jats:italic>= 2683.3 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.035, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.096, <jats:italic>T </jats:italic>= 193 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>N<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>Sn, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.606(7) Å, <jats:italic>b </jats:italic>= 19.842(9) Å, <jats:italic>c </jats:italic>= 15.129(9) Å, β = 98.91(2)°, <jats:italic>V </jats:italic>= 2848.8 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.038, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.089, <jats:italic>T </jats:italic>= 300 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>MoN<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.505(3) Å, <jats:italic>b </jats:italic>= 19.624(2) Å, <jats:italic>c </jats:italic>= 14.759(2) Å, β = 98.72(2)°, <jats:italic>V </jats:italic>= 2721.1 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.062, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.175, <jats:italic>T </jats:italic>= 193 K.</jats:p> Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) Zeitschrift für Kristallographie - New Crystal Structures |
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Walter de Gruyter GmbH, 2004 |
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Walter de Gruyter GmbH, 2004 |
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2197-4578 1433-7266 |
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2197-4578 1433-7266 |
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rabe2004crystalstructuresofacetonitrilesolvatesofbistetraphenylphosphoniumtetrachlorooxovanadateivhexachlorostannateivandmolybdateivpc6h542vocl44ch3cnpc6h542mcl64ch3cnmsnmo |
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Zeitschrift für Kristallographie - New Crystal Structures |
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49 |
| title |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_unstemmed |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_full |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_fullStr |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_full_unstemmed |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_short |
Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_sort |
crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(iv), hexachlorostannate(iv) and -molybdate(iv), [p(c6h5)4]2[vocl4] · 4ch3cn, [p(c6h5)4]2[mcl6] · 4ch3cn (m = sn, mo) |
| topic |
Inorganic Chemistry Condensed Matter Physics General Materials Science |
| url |
http://dx.doi.org/10.1524/ncrs.2004.219.2.101 |
| publishDate |
2004 |
| physical |
101-105 |
| description |
<jats:title>Abstract</jats:title><jats:p> C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>4</jats:sub>N<jats:sub>4</jats:sub>OP<jats:sub>2</jats:sub>V, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.473(2) Å, <jats:italic>b </jats:italic>= 19.832(6) Å, <jats:italic>c </jats:italic>= 14.461(2) Å, β = 99.00(2)°, <jats:italic>V </jats:italic>= 2683.3 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.035, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.096, <jats:italic>T </jats:italic>= 193 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>N<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>Sn, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.606(7) Å, <jats:italic>b </jats:italic>= 19.842(9) Å, <jats:italic>c </jats:italic>= 15.129(9) Å, β = 98.91(2)°, <jats:italic>V </jats:italic>= 2848.8 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.038, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.089, <jats:italic>T </jats:italic>= 300 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>MoN<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.505(3) Å, <jats:italic>b </jats:italic>= 19.624(2) Å, <jats:italic>c </jats:italic>= 14.759(2) Å, β = 98.72(2)°, <jats:italic>V </jats:italic>= 2721.1 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.062, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.175, <jats:italic>T </jats:italic>= 193 K.</jats:p> |
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| series | Zeitschrift für Kristallographie - New Crystal Structures |
| source_id | 49 |
| spelling | Rabe, Susanne Bubenheim, Wilfried Müller, Ulrich 2197-4578 1433-7266 Walter de Gruyter GmbH Inorganic Chemistry Condensed Matter Physics General Materials Science http://dx.doi.org/10.1524/ncrs.2004.219.2.101 <jats:title>Abstract</jats:title><jats:p> C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>4</jats:sub>N<jats:sub>4</jats:sub>OP<jats:sub>2</jats:sub>V, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.473(2) Å, <jats:italic>b </jats:italic>= 19.832(6) Å, <jats:italic>c </jats:italic>= 14.461(2) Å, β = 99.00(2)°, <jats:italic>V </jats:italic>= 2683.3 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.035, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.096, <jats:italic>T </jats:italic>= 193 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>N<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>Sn, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.606(7) Å, <jats:italic>b </jats:italic>= 19.842(9) Å, <jats:italic>c </jats:italic>= 15.129(9) Å, β = 98.91(2)°, <jats:italic>V </jats:italic>= 2848.8 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.038, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.089, <jats:italic>T </jats:italic>= 300 K.</jats:p><jats:p>C<jats:sub>56</jats:sub>H<jats:sub>52</jats:sub>Cl<jats:sub>6</jats:sub>MoN<jats:sub>4</jats:sub>P<jats:sub>2</jats:sub>, monoclinic, <jats:italic>P</jats:italic>12<jats:sub>1</jats:sub>/<jats:italic>c</jats:italic>1 (no. 14), <jats:italic>a </jats:italic>= 9.505(3) Å, <jats:italic>b </jats:italic>= 19.624(2) Å, <jats:italic>c </jats:italic>= 14.759(2) Å, β = 98.72(2)°, <jats:italic>V </jats:italic>= 2721.1 Å<jats:sup>3</jats:sup>, <jats:italic>Z </jats:italic>= 2, <jats:italic>R</jats:italic><jats:sub>gt</jats:sub><jats:italic>(F) </jats:italic>= 0.062, <jats:italic>wR</jats:italic><jats:sub>ref</jats:sub><jats:italic>(F</jats:italic><jats:sup>2</jats:sup><jats:italic>) </jats:italic>= 0.175, <jats:italic>T </jats:italic>= 193 K.</jats:p> Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) Zeitschrift für Kristallographie - New Crystal Structures |
| spellingShingle | Rabe, Susanne, Bubenheim, Wilfried, Müller, Ulrich, Zeitschrift für Kristallographie - New Crystal Structures, Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo), Inorganic Chemistry, Condensed Matter Physics, General Materials Science |
| title | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_full | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_fullStr | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_full_unstemmed | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_short | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| title_sort | crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(iv), hexachlorostannate(iv) and -molybdate(iv), [p(c6h5)4]2[vocl4] · 4ch3cn, [p(c6h5)4]2[mcl6] · 4ch3cn (m = sn, mo) |
| title_unstemmed | Crystal structures of acetonitrile solvates of bis(tetraphenylphosphonium) tetrachlorooxovanadate(IV), hexachlorostannate(IV) and -molybdate(IV), [P(C6H5)4]2[VOCl4] · 4CH3CN, [P(C6H5)4]2[MCl6] · 4CH3CN (M = Sn, Mo) |
| topic | Inorganic Chemistry, Condensed Matter Physics, General Materials Science |
| url | http://dx.doi.org/10.1524/ncrs.2004.219.2.101 |