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Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazin...
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| Zeitschriftentitel: | Zeitschrift für Naturforschung B |
|---|---|
| Personen und Körperschaften: | , , |
| In: | Zeitschrift für Naturforschung B, 52, 1997, 1, S. 138-140 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Walter de Gruyter GmbH
|
| Schlagwörter: |
| author_facet |
Kunkel, Frank Harms, Klaus Dehnicke, Kurt Kunkel, Frank Harms, Klaus Dehnicke, Kurt |
|---|---|
| author |
Kunkel, Frank Harms, Klaus Dehnicke, Kurt |
| spellingShingle |
Kunkel, Frank Harms, Klaus Dehnicke, Kurt Zeitschrift für Naturforschung B Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 General Chemistry |
| author_sort |
kunkel, frank |
| spelling |
Kunkel, Frank Harms, Klaus Dehnicke, Kurt 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-1997-0126 <jats:p>Single crystals of [WCl<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> were obtained by the reaction of triphenyl-cycIo-1λ<jats:sup>5</jats:sup>antimonia-2,4-dithia-3,5-diazine, SbPh<jats:sub>3</jats:sub>(N<jats:sub>2</jats:sub>S<jats:sub>2</jats:sub>), with tungsten hexachloride in dichloromethane. Space group P2<jats:sub>1</jats:sub>/n, Z = 2, lattice dimensions at -80°C: a = 744.8(1), b = 923.5(1), c = 1078.7(1) pm, β = 94.43(1)°, R = 0.036. [WCI<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> forms centrosymmetric molecules with W<jats:sub>2</jats:sub>N<jats:sub>2</jats:sub>-fourmembered rings and planar cyclo-WN<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub> units</jats:p> Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ<sup>6</sup>-wolframa-3,5-dithia-2,4,6- triazin, [WCl<sub>3</sub>(N<sub>3</sub>S<sub>2</sub> )]<sub>2</sub> / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ<sup>6</sup>-tungsta-3,5-dithia-2,4,6-triazine, [WCl<sub>3</sub>(N<sub>3</sub>S<sub>2</sub>)]<sub>2</sub> Zeitschrift für Naturforschung B |
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10.1515/znb-1997-0126 |
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Walter de Gruyter GmbH, 1997 |
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Walter de Gruyter GmbH, 1997 |
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1865-7117 0932-0776 |
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1865-7117 0932-0776 |
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Walter de Gruyter GmbH (CrossRef) |
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| title |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_unstemmed |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_full |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_fullStr |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_full_unstemmed |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_short |
Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_sort |
kristallstruktur von 1,1,1-trichloro-cyclo-1λ<sup>6</sup>-wolframa-3,5-dithia-2,4,6- triazin, [wcl<sub>3</sub>(n<sub>3</sub>s<sub>2</sub> )]<sub>2</sub> / crystal structure of 1,1,1-trichloro-cyclo- 1λ<sup>6</sup>-tungsta-3,5-dithia-2,4,6-triazine, [wcl<sub>3</sub>(n<sub>3</sub>s<sub>2</sub>)]<sub>2</sub> |
| topic |
General Chemistry |
| url |
http://dx.doi.org/10.1515/znb-1997-0126 |
| publishDate |
1997 |
| physical |
138-140 |
| description |
<jats:p>Single crystals of [WCl<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> were obtained by the reaction of triphenyl-cycIo-1λ<jats:sup>5</jats:sup>antimonia-2,4-dithia-3,5-diazine, SbPh<jats:sub>3</jats:sub>(N<jats:sub>2</jats:sub>S<jats:sub>2</jats:sub>), with tungsten hexachloride in dichloromethane. Space group P2<jats:sub>1</jats:sub>/n, Z = 2, lattice dimensions at -80°C: a = 744.8(1), b = 923.5(1), c = 1078.7(1) pm, β = 94.43(1)°, R = 0.036. [WCI<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> forms centrosymmetric molecules with W<jats:sub>2</jats:sub>N<jats:sub>2</jats:sub>-fourmembered rings and planar cyclo-WN<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub> units</jats:p> |
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url_ver=Z39.88-2004&ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fvufind.svn.sourceforge.net%3Agenerator&rft.title=Kristallstruktur+von+1%2C1%2C1-Trichloro-cyclo-1%CE%BB6-wolframa-3%2C5-dithia-2%2C4%2C6-+triazin%2C+%5BWCl3%28N3S2+%29%5D2+%2F+Crystal+Structure+of+1%2C1%2C1-Trichloro-cyclo-+1%CE%BB6-tungsta-3%2C5-dithia-2%2C4%2C6-triazine%2C+%5BWCl3%28N3S2%29%5D2&rft.date=1997-01-01&genre=article&issn=0932-0776&volume=52&issue=1&spage=138&epage=140&pages=138-140&jtitle=Zeitschrift+f%C3%BCr+Naturforschung+B&atitle=Kristallstruktur+von+1%2C1%2C1-Trichloro-cyclo-1%CE%BB%3Csup%3E6%3C%2Fsup%3E-wolframa-3%2C5-dithia-2%2C4%2C6-+triazin%2C+%5BWCl%3Csub%3E3%3C%2Fsub%3E%28N%3Csub%3E3%3C%2Fsub%3ES%3Csub%3E2%3C%2Fsub%3E+%29%5D%3Csub%3E2%3C%2Fsub%3E+%2F+Crystal+Structure+of+1%2C1%2C1-Trichloro-cyclo-+1%CE%BB%3Csup%3E6%3C%2Fsup%3E-tungsta-3%2C5-dithia-2%2C4%2C6-triazine%2C+%5BWCl%3Csub%3E3%3C%2Fsub%3E%28N%3Csub%3E3%3C%2Fsub%3ES%3Csub%3E2%3C%2Fsub%3E%29%5D%3Csub%3E2%3C%2Fsub%3E&aulast=Dehnicke&aufirst=Kurt&rft_id=info%3Adoi%2F10.1515%2Fznb-1997-0126&rft.language%5B0%5D=eng |
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| author | Kunkel, Frank, Harms, Klaus, Dehnicke, Kurt |
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| description | <jats:p>Single crystals of [WCl<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> were obtained by the reaction of triphenyl-cycIo-1λ<jats:sup>5</jats:sup>antimonia-2,4-dithia-3,5-diazine, SbPh<jats:sub>3</jats:sub>(N<jats:sub>2</jats:sub>S<jats:sub>2</jats:sub>), with tungsten hexachloride in dichloromethane. Space group P2<jats:sub>1</jats:sub>/n, Z = 2, lattice dimensions at -80°C: a = 744.8(1), b = 923.5(1), c = 1078.7(1) pm, β = 94.43(1)°, R = 0.036. [WCI<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> forms centrosymmetric molecules with W<jats:sub>2</jats:sub>N<jats:sub>2</jats:sub>-fourmembered rings and planar cyclo-WN<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub> units</jats:p> |
| doi_str_mv | 10.1515/znb-1997-0126 |
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| imprint | Walter de Gruyter GmbH, 1997 |
| imprint_str_mv | Walter de Gruyter GmbH, 1997 |
| institution | DE-D275, DE-Bn3, DE-Brt1, DE-D161, DE-Zwi2, DE-Gla1, DE-Zi4, DE-15, DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229 |
| issn | 1865-7117, 0932-0776 |
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| language | English |
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| match_str | kunkel1997kristallstrukturvon111trichlorocyclo1l6wolframa35dithia246triazinwcl3n3s22crystalstructureof111trichlorocyclo1l6tungsta35dithia246triazinewcl3n3s22 |
| mega_collection | Walter de Gruyter GmbH (CrossRef) |
| physical | 138-140 |
| publishDate | 1997 |
| publishDateSort | 1997 |
| publisher | Walter de Gruyter GmbH |
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| series | Zeitschrift für Naturforschung B |
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| spelling | Kunkel, Frank Harms, Klaus Dehnicke, Kurt 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-1997-0126 <jats:p>Single crystals of [WCl<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> were obtained by the reaction of triphenyl-cycIo-1λ<jats:sup>5</jats:sup>antimonia-2,4-dithia-3,5-diazine, SbPh<jats:sub>3</jats:sub>(N<jats:sub>2</jats:sub>S<jats:sub>2</jats:sub>), with tungsten hexachloride in dichloromethane. Space group P2<jats:sub>1</jats:sub>/n, Z = 2, lattice dimensions at -80°C: a = 744.8(1), b = 923.5(1), c = 1078.7(1) pm, β = 94.43(1)°, R = 0.036. [WCI<jats:sub>3</jats:sub>(N<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub>)]<jats:sub>2</jats:sub> forms centrosymmetric molecules with W<jats:sub>2</jats:sub>N<jats:sub>2</jats:sub>-fourmembered rings and planar cyclo-WN<jats:sub>3</jats:sub>S<jats:sub>2</jats:sub> units</jats:p> Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ<sup>6</sup>-wolframa-3,5-dithia-2,4,6- triazin, [WCl<sub>3</sub>(N<sub>3</sub>S<sub>2</sub> )]<sub>2</sub> / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ<sup>6</sup>-tungsta-3,5-dithia-2,4,6-triazine, [WCl<sub>3</sub>(N<sub>3</sub>S<sub>2</sub>)]<sub>2</sub> Zeitschrift für Naturforschung B |
| spellingShingle | Kunkel, Frank, Harms, Klaus, Dehnicke, Kurt, Zeitschrift für Naturforschung B, Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2, General Chemistry |
| title | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_full | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_fullStr | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_full_unstemmed | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_short | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| title_sort | kristallstruktur von 1,1,1-trichloro-cyclo-1λ<sup>6</sup>-wolframa-3,5-dithia-2,4,6- triazin, [wcl<sub>3</sub>(n<sub>3</sub>s<sub>2</sub> )]<sub>2</sub> / crystal structure of 1,1,1-trichloro-cyclo- 1λ<sup>6</sup>-tungsta-3,5-dithia-2,4,6-triazine, [wcl<sub>3</sub>(n<sub>3</sub>s<sub>2</sub>)]<sub>2</sub> |
| title_unstemmed | Kristallstruktur von 1,1,1-Trichloro-cyclo-1λ6-wolframa-3,5-dithia-2,4,6- triazin, [WCl3(N3S2 )]2 / Crystal Structure of 1,1,1-Trichloro-cyclo- 1λ6-tungsta-3,5-dithia-2,4,6-triazine, [WCl3(N3S2)]2 |
| topic | General Chemistry |
| url | http://dx.doi.org/10.1515/znb-1997-0126 |