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Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—...

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Zeitschriftentitel: Zeitschrift für Naturforschung B
Personen und Körperschaften: Hönle, Wolfgang, Walz, Leonhard, Schnering, Hans Georg von
In: Zeitschrift für Naturforschung B, 45, 1990, 9, S. 1251-1254
Format: E-Article
Sprache: Englisch
veröffentlicht:
Walter de Gruyter GmbH
Schlagwörter:
General Chemistry
author_facet Hönle, Wolfgang
Walz, Leonhard
Schnering, Hans Georg von
Hönle, Wolfgang
Walz, Leonhard
Schnering, Hans Georg von
author Hönle, Wolfgang
Walz, Leonhard
Schnering, Hans Georg von
spellingShingle Hönle, Wolfgang
Walz, Leonhard
Schnering, Hans Georg von
Zeitschrift für Naturforschung B
Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
General Chemistry
author_sort hönle, wolfgang
spelling Hönle, Wolfgang Walz, Leonhard Schnering, Hans Georg von 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-1990-0905 <jats:p>Ethylenediammonium Hydridotrioxophosphate(2–) [H<jats:sub>3</jats:sub>NCH<jats:sub>2</jats:sub>CH<jats:sub>2</jats:sub>NH<jats:sub>3</jats:sub>][PHO<jats:sub>3</jats:sub>] is formed by slow oxidation of white phosphorus by oxygen in ethylendiamine. It crystallizes in the space group Pbca with a = 1570.6(4) pm, b = 676.9(5) pm, c = 1267.8(4) pm and Z = 8 formula units in the unit cell. The structure is built from ethylenediammonium dications and tetrahedral phosphonate dianions, linked by O ··· H–N bonds (d̄(O…N) = 275.8 pm). The bond distances are d̄(P–O) = 151.8 pm, d̄(P–H) = 136.9 pm, d̄(N–C) = 148.3 pm and d̄(C–C) = 151.0 pm.</jats:p> Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H<sub>3</sub>NCH<sub>2</sub>CH<sub>2</sub>NH<sub>3</sub>][PHO<sub>3</sub>]<sup>a</sup> / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H<sub>3</sub>NCH<sub>2</sub>CH<sub>2</sub>NH<sub>3</sub>][PHO<sub>3</sub>] Zeitschrift für Naturforschung B
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publishDateSort 1990
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source_id 49
title Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_unstemmed Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_full Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_fullStr Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_full_unstemmed Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_short Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_sort bildung und kristallstruktur von ethylendiammonium-hydridotrioxophosphat(2–) [h<sub>3</sub>nch<sub>2</sub>ch<sub>2</sub>nh<sub>3</sub>][pho<sub>3</sub>]<sup>a</sup> / formation and crystal structure of ethylenediammonium hydridotrioxophosphate(2—) [h<sub>3</sub>nch<sub>2</sub>ch<sub>2</sub>nh<sub>3</sub>][pho<sub>3</sub>]
topic General Chemistry
url http://dx.doi.org/10.1515/znb-1990-0905
publishDate 1990
physical 1251-1254
description <jats:p>Ethylenediammonium Hydridotrioxophosphate(2–) [H<jats:sub>3</jats:sub>NCH<jats:sub>2</jats:sub>CH<jats:sub>2</jats:sub>NH<jats:sub>3</jats:sub>][PHO<jats:sub>3</jats:sub>] is formed by slow oxidation of white phosphorus by oxygen in ethylendiamine. It crystallizes in the space group Pbca with a = 1570.6(4) pm, b = 676.9(5) pm, c = 1267.8(4) pm and Z = 8 formula units in the unit cell. The structure is built from ethylenediammonium dications and tetrahedral phosphonate dianions, linked by O ··· H–N bonds (d̄(O…N) = 275.8 pm). The bond distances are d̄(P–O) = 151.8 pm, d̄(P–H) = 136.9 pm, d̄(N–C) = 148.3 pm and d̄(C–C) = 151.0 pm.</jats:p>
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author Hönle, Wolfgang, Walz, Leonhard, Schnering, Hans Georg von
author_facet Hönle, Wolfgang, Walz, Leonhard, Schnering, Hans Georg von, Hönle, Wolfgang, Walz, Leonhard, Schnering, Hans Georg von
author_sort hönle, wolfgang
container_issue 9
container_start_page 1251
container_title Zeitschrift für Naturforschung B
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description <jats:p>Ethylenediammonium Hydridotrioxophosphate(2–) [H<jats:sub>3</jats:sub>NCH<jats:sub>2</jats:sub>CH<jats:sub>2</jats:sub>NH<jats:sub>3</jats:sub>][PHO<jats:sub>3</jats:sub>] is formed by slow oxidation of white phosphorus by oxygen in ethylendiamine. It crystallizes in the space group Pbca with a = 1570.6(4) pm, b = 676.9(5) pm, c = 1267.8(4) pm and Z = 8 formula units in the unit cell. The structure is built from ethylenediammonium dications and tetrahedral phosphonate dianions, linked by O ··· H–N bonds (d̄(O…N) = 275.8 pm). The bond distances are d̄(P–O) = 151.8 pm, d̄(P–H) = 136.9 pm, d̄(N–C) = 148.3 pm and d̄(C–C) = 151.0 pm.</jats:p>
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imprint_str_mv Walter de Gruyter GmbH, 1990
institution DE-D275, DE-Bn3, DE-Brt1, DE-Zwi2, DE-D161, DE-Gla1, DE-Zi4, DE-15, DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229
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spelling Hönle, Wolfgang Walz, Leonhard Schnering, Hans Georg von 1865-7117 0932-0776 Walter de Gruyter GmbH General Chemistry http://dx.doi.org/10.1515/znb-1990-0905 <jats:p>Ethylenediammonium Hydridotrioxophosphate(2–) [H<jats:sub>3</jats:sub>NCH<jats:sub>2</jats:sub>CH<jats:sub>2</jats:sub>NH<jats:sub>3</jats:sub>][PHO<jats:sub>3</jats:sub>] is formed by slow oxidation of white phosphorus by oxygen in ethylendiamine. It crystallizes in the space group Pbca with a = 1570.6(4) pm, b = 676.9(5) pm, c = 1267.8(4) pm and Z = 8 formula units in the unit cell. The structure is built from ethylenediammonium dications and tetrahedral phosphonate dianions, linked by O ··· H–N bonds (d̄(O…N) = 275.8 pm). The bond distances are d̄(P–O) = 151.8 pm, d̄(P–H) = 136.9 pm, d̄(N–C) = 148.3 pm and d̄(C–C) = 151.0 pm.</jats:p> Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H<sub>3</sub>NCH<sub>2</sub>CH<sub>2</sub>NH<sub>3</sub>][PHO<sub>3</sub>]<sup>a</sup> / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H<sub>3</sub>NCH<sub>2</sub>CH<sub>2</sub>NH<sub>3</sub>][PHO<sub>3</sub>] Zeitschrift für Naturforschung B
spellingShingle Hönle, Wolfgang, Walz, Leonhard, Schnering, Hans Georg von, Zeitschrift für Naturforschung B, Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3], General Chemistry
title Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_full Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_fullStr Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_full_unstemmed Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_short Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
title_sort bildung und kristallstruktur von ethylendiammonium-hydridotrioxophosphat(2–) [h<sub>3</sub>nch<sub>2</sub>ch<sub>2</sub>nh<sub>3</sub>][pho<sub>3</sub>]<sup>a</sup> / formation and crystal structure of ethylenediammonium hydridotrioxophosphate(2—) [h<sub>3</sub>nch<sub>2</sub>ch<sub>2</sub>nh<sub>3</sub>][pho<sub>3</sub>]
title_unstemmed Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H3NCH2CH2NH3][PHO3]a / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H3NCH2CH2NH3][PHO3]
topic General Chemistry
url http://dx.doi.org/10.1515/znb-1990-0905