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Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate
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| Zeitschriftentitel: | Acta Crystallographica Section E Crystallographic Communications |
|---|---|
| Personen und Körperschaften: | , |
| In: | Acta Crystallographica Section E Crystallographic Communications, 72, 2016, 4, S. 467-469 |
| Format: | E-Article |
| Sprache: | Unbestimmt |
| veröffentlicht: |
International Union of Crystallography (IUCr)
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| Schlagwörter: |
| author_facet |
Li, Wen-Juan Han, Hong-Fei Li, Wen-Juan Han, Hong-Fei |
|---|---|
| author |
Li, Wen-Juan Han, Hong-Fei |
| spellingShingle |
Li, Wen-Juan Han, Hong-Fei Acta Crystallographica Section E Crystallographic Communications Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate Condensed Matter Physics General Materials Science General Chemistry |
| author_sort |
li, wen-juan |
| spelling |
Li, Wen-Juan Han, Hong-Fei 2056-9890 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s2056989016003686 <jats:p>In the title compound {systematic name: 4,4′-[1,1′-(hydrazinediylidene)bis(ethan-1-yl-1-ylidene)]bis(benzene-1,3-diol)}, C<jats:sub>16</jats:sub>H<jats:sub>16</jats:sub>N<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub>·2C<jats:sub>3</jats:sub>H<jats:sub>7</jats:sub>NO, the (<jats:italic>E</jats:italic>,<jats:italic>E</jats:italic>)-2′,4′-dihydroxyacetophenone azine molecule is centrosymmetric, the mid-point of the N—N bond being located on an inversion centre. All the non-H atoms of the azine molecule are approximately coplanar, the maximum deviation being 0.017 (2) Å. An intramolecular O—H...N hydrogen bond occurs between the azine N atom and the hydroxy group. In the crystal, azine and dimethylformamide solvent molecules are linked by O—H...O hydrogen bonds.</jats:p> Crystal structure of (<i>E</i>,<i>E</i>)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate Acta Crystallographica Section E Crystallographic Communications |
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International Union of Crystallography (IUCr), 2016 |
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International Union of Crystallography (IUCr), 2016 |
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Acta Crystallographica Section E Crystallographic Communications |
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| title |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_unstemmed |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_full |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_fullStr |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_full_unstemmed |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_short |
Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_sort |
crystal structure of (<i>e</i>,<i>e</i>)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| topic |
Condensed Matter Physics General Materials Science General Chemistry |
| url |
http://dx.doi.org/10.1107/s2056989016003686 |
| publishDate |
2016 |
| physical |
467-469 |
| description |
<jats:p>In the title compound {systematic name: 4,4′-[1,1′-(hydrazinediylidene)bis(ethan-1-yl-1-ylidene)]bis(benzene-1,3-diol)}, C<jats:sub>16</jats:sub>H<jats:sub>16</jats:sub>N<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub>·2C<jats:sub>3</jats:sub>H<jats:sub>7</jats:sub>NO, the (<jats:italic>E</jats:italic>,<jats:italic>E</jats:italic>)-2′,4′-dihydroxyacetophenone azine molecule is centrosymmetric, the mid-point of the N—N bond being located on an inversion centre. All the non-H atoms of the azine molecule are approximately coplanar, the maximum deviation being 0.017 (2) Å. An intramolecular O—H...N hydrogen bond occurs between the azine N atom and the hydroxy group. In the crystal, azine and dimethylformamide solvent molecules are linked by O—H...O hydrogen bonds.</jats:p> |
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| author | Li, Wen-Juan, Han, Hong-Fei |
| author_facet | Li, Wen-Juan, Han, Hong-Fei, Li, Wen-Juan, Han, Hong-Fei |
| author_sort | li, wen-juan |
| container_issue | 4 |
| container_start_page | 467 |
| container_title | Acta Crystallographica Section E Crystallographic Communications |
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| description | <jats:p>In the title compound {systematic name: 4,4′-[1,1′-(hydrazinediylidene)bis(ethan-1-yl-1-ylidene)]bis(benzene-1,3-diol)}, C<jats:sub>16</jats:sub>H<jats:sub>16</jats:sub>N<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub>·2C<jats:sub>3</jats:sub>H<jats:sub>7</jats:sub>NO, the (<jats:italic>E</jats:italic>,<jats:italic>E</jats:italic>)-2′,4′-dihydroxyacetophenone azine molecule is centrosymmetric, the mid-point of the N—N bond being located on an inversion centre. All the non-H atoms of the azine molecule are approximately coplanar, the maximum deviation being 0.017 (2) Å. An intramolecular O—H...N hydrogen bond occurs between the azine N atom and the hydroxy group. In the crystal, azine and dimethylformamide solvent molecules are linked by O—H...O hydrogen bonds.</jats:p> |
| doi_str_mv | 10.1107/s2056989016003686 |
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| imprint | International Union of Crystallography (IUCr), 2016 |
| imprint_str_mv | International Union of Crystallography (IUCr), 2016 |
| institution | DE-Gla1, DE-Zi4, DE-15, DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229, DE-D275, DE-Bn3, DE-Brt1, DE-Zwi2, DE-D161 |
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| physical | 467-469 |
| publishDate | 2016 |
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| publisher | International Union of Crystallography (IUCr) |
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| series | Acta Crystallographica Section E Crystallographic Communications |
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| spelling | Li, Wen-Juan Han, Hong-Fei 2056-9890 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s2056989016003686 <jats:p>In the title compound {systematic name: 4,4′-[1,1′-(hydrazinediylidene)bis(ethan-1-yl-1-ylidene)]bis(benzene-1,3-diol)}, C<jats:sub>16</jats:sub>H<jats:sub>16</jats:sub>N<jats:sub>2</jats:sub>O<jats:sub>4</jats:sub>·2C<jats:sub>3</jats:sub>H<jats:sub>7</jats:sub>NO, the (<jats:italic>E</jats:italic>,<jats:italic>E</jats:italic>)-2′,4′-dihydroxyacetophenone azine molecule is centrosymmetric, the mid-point of the N—N bond being located on an inversion centre. All the non-H atoms of the azine molecule are approximately coplanar, the maximum deviation being 0.017 (2) Å. An intramolecular O—H...N hydrogen bond occurs between the azine N atom and the hydroxy group. In the crystal, azine and dimethylformamide solvent molecules are linked by O—H...O hydrogen bonds.</jats:p> Crystal structure of (<i>E</i>,<i>E</i>)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate Acta Crystallographica Section E Crystallographic Communications |
| spellingShingle | Li, Wen-Juan, Han, Hong-Fei, Acta Crystallographica Section E Crystallographic Communications, Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate, Condensed Matter Physics, General Materials Science, General Chemistry |
| title | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_full | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_fullStr | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_full_unstemmed | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_short | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_sort | crystal structure of (<i>e</i>,<i>e</i>)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| title_unstemmed | Crystal structure of (E,E)-2′,4′-dihydroxyacetophenone azine dimethylformamide disolvate |
| topic | Condensed Matter Physics, General Materials Science, General Chemistry |
| url | http://dx.doi.org/10.1107/s2056989016003686 |