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Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2)
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| Zeitschriftentitel: | Acta Crystallographica Section E Structure Reports Online |
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| Personen und Körperschaften: | , , , |
| In: | Acta Crystallographica Section E Structure Reports Online, 70, 2014, 1, S. m7-m8 |
| Format: | E-Article |
| Sprache: | Unbestimmt |
| veröffentlicht: |
International Union of Crystallography (IUCr)
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| Schlagwörter: |
| author_facet |
Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti |
|---|---|
| author |
Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti |
| spellingShingle |
Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti Acta Crystallographica Section E Structure Reports Online Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) Condensed Matter Physics General Materials Science General Chemistry |
| author_sort |
bulatov, evgeny |
| spelling |
Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti 1600-5368 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s1600536813032649 <jats:p>In the title complex, (NH<jats:sub>3</jats:sub>OH)<jats:sub>2</jats:sub>[PtCl<jats:sub>6</jats:sub>]·2C<jats:sub>12</jats:sub>H<jats:sub>24</jats:sub>O<jats:sub>6</jats:sub>, the Pt<jats:sup>IV</jats:sup> atom is coordinated by six chloride anions in a slightly distorted octahedral geometry. The Pt—Cl bond lengths are comparable to those reported for other hexachloridoplatinate(IV) species. The hydroxyammonium groups act as linkers between the [PtCl<jats:sub>6</jats:sub>]<jats:sup>2−</jats:sup> anion and the crown ether molecules. The anion is linked to two hydroxyammonium cations <jats:italic>via</jats:italic> O—H...Cl hydrogen bonds and each hydroxyammonium moiety is linked to a crown ether molecule by hydrogen bonds between ammonium H atoms and 18-crown-6 O atoms. The crown ether molecules have the classic crown shape in which all O atoms are located in the inner part of the crown ether ring and all –CH<jats:sub>2</jats:sub>– groups are turned to the outside.</jats:p> Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) Acta Crystallographica Section E Structure Reports Online |
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10.1107/s1600536813032649 |
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DE-15 DE-Pl11 DE-Rs1 DE-105 DE-14 DE-Ch1 DE-L229 DE-D275 DE-Bn3 DE-Brt1 DE-Zwi2 DE-D161 DE-Gla1 DE-Zi4 |
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International Union of Crystallography (IUCr), 2014 |
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International Union of Crystallography (IUCr), 2014 |
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1600-5368 |
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International Union of Crystallography (IUCr) (CrossRef) |
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Acta Crystallographica Section E Structure Reports Online |
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49 |
| title |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_unstemmed |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_full |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_fullStr |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_full_unstemmed |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_short |
Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_sort |
bis(hydroxyammonium) hexachloridoplatinate(iv)–18-crown-6 (1/2) |
| topic |
Condensed Matter Physics General Materials Science General Chemistry |
| url |
http://dx.doi.org/10.1107/s1600536813032649 |
| publishDate |
2014 |
| physical |
m7-m8 |
| description |
<jats:p>In the title complex, (NH<jats:sub>3</jats:sub>OH)<jats:sub>2</jats:sub>[PtCl<jats:sub>6</jats:sub>]·2C<jats:sub>12</jats:sub>H<jats:sub>24</jats:sub>O<jats:sub>6</jats:sub>, the Pt<jats:sup>IV</jats:sup> atom is coordinated by six chloride anions in a slightly distorted octahedral geometry. The Pt—Cl bond lengths are comparable to those reported for other hexachloridoplatinate(IV) species. The hydroxyammonium groups act as linkers between the [PtCl<jats:sub>6</jats:sub>]<jats:sup>2−</jats:sup> anion and the crown ether molecules. The anion is linked to two hydroxyammonium cations <jats:italic>via</jats:italic> O—H...Cl hydrogen bonds and each hydroxyammonium moiety is linked to a crown ether molecule by hydrogen bonds between ammonium H atoms and 18-crown-6 O atoms. The crown ether molecules have the classic crown shape in which all O atoms are located in the inner part of the crown ether ring and all –CH<jats:sub>2</jats:sub>– groups are turned to the outside.</jats:p> |
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| author | Bulatov, Evgeny, Afanasenko, Anastasiya, Chulkova, Tatiana, Haukka, Matti |
| author_facet | Bulatov, Evgeny, Afanasenko, Anastasiya, Chulkova, Tatiana, Haukka, Matti, Bulatov, Evgeny, Afanasenko, Anastasiya, Chulkova, Tatiana, Haukka, Matti |
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| description | <jats:p>In the title complex, (NH<jats:sub>3</jats:sub>OH)<jats:sub>2</jats:sub>[PtCl<jats:sub>6</jats:sub>]·2C<jats:sub>12</jats:sub>H<jats:sub>24</jats:sub>O<jats:sub>6</jats:sub>, the Pt<jats:sup>IV</jats:sup> atom is coordinated by six chloride anions in a slightly distorted octahedral geometry. The Pt—Cl bond lengths are comparable to those reported for other hexachloridoplatinate(IV) species. The hydroxyammonium groups act as linkers between the [PtCl<jats:sub>6</jats:sub>]<jats:sup>2−</jats:sup> anion and the crown ether molecules. The anion is linked to two hydroxyammonium cations <jats:italic>via</jats:italic> O—H...Cl hydrogen bonds and each hydroxyammonium moiety is linked to a crown ether molecule by hydrogen bonds between ammonium H atoms and 18-crown-6 O atoms. The crown ether molecules have the classic crown shape in which all O atoms are located in the inner part of the crown ether ring and all –CH<jats:sub>2</jats:sub>– groups are turned to the outside.</jats:p> |
| doi_str_mv | 10.1107/s1600536813032649 |
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| imprint | International Union of Crystallography (IUCr), 2014 |
| imprint_str_mv | International Union of Crystallography (IUCr), 2014 |
| institution | DE-15, DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229, DE-D275, DE-Bn3, DE-Brt1, DE-Zwi2, DE-D161, DE-Gla1, DE-Zi4 |
| issn | 1600-5368 |
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| mega_collection | International Union of Crystallography (IUCr) (CrossRef) |
| physical | m7-m8 |
| publishDate | 2014 |
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| publisher | International Union of Crystallography (IUCr) |
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| series | Acta Crystallographica Section E Structure Reports Online |
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| spelling | Bulatov, Evgeny Afanasenko, Anastasiya Chulkova, Tatiana Haukka, Matti 1600-5368 International Union of Crystallography (IUCr) Condensed Matter Physics General Materials Science General Chemistry http://dx.doi.org/10.1107/s1600536813032649 <jats:p>In the title complex, (NH<jats:sub>3</jats:sub>OH)<jats:sub>2</jats:sub>[PtCl<jats:sub>6</jats:sub>]·2C<jats:sub>12</jats:sub>H<jats:sub>24</jats:sub>O<jats:sub>6</jats:sub>, the Pt<jats:sup>IV</jats:sup> atom is coordinated by six chloride anions in a slightly distorted octahedral geometry. The Pt—Cl bond lengths are comparable to those reported for other hexachloridoplatinate(IV) species. The hydroxyammonium groups act as linkers between the [PtCl<jats:sub>6</jats:sub>]<jats:sup>2−</jats:sup> anion and the crown ether molecules. The anion is linked to two hydroxyammonium cations <jats:italic>via</jats:italic> O—H...Cl hydrogen bonds and each hydroxyammonium moiety is linked to a crown ether molecule by hydrogen bonds between ammonium H atoms and 18-crown-6 O atoms. The crown ether molecules have the classic crown shape in which all O atoms are located in the inner part of the crown ether ring and all –CH<jats:sub>2</jats:sub>– groups are turned to the outside.</jats:p> Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) Acta Crystallographica Section E Structure Reports Online |
| spellingShingle | Bulatov, Evgeny, Afanasenko, Anastasiya, Chulkova, Tatiana, Haukka, Matti, Acta Crystallographica Section E Structure Reports Online, Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2), Condensed Matter Physics, General Materials Science, General Chemistry |
| title | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_full | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_fullStr | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_full_unstemmed | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_short | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| title_sort | bis(hydroxyammonium) hexachloridoplatinate(iv)–18-crown-6 (1/2) |
| title_unstemmed | Bis(hydroxyammonium) hexachloridoplatinate(IV)–18-crown-6 (1/2) |
| topic | Condensed Matter Physics, General Materials Science, General Chemistry |
| url | http://dx.doi.org/10.1107/s1600536813032649 |