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Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions
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| Zeitschriftentitel: | Journal of Labelled Compounds and Radiopharmaceuticals |
|---|---|
| Personen und Körperschaften: | , |
| In: | Journal of Labelled Compounds and Radiopharmaceuticals, 19, 1982, 1, S. 151-153 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Wiley
|
| Schlagwörter: |
| author_facet |
Chung, S. K. Hansen, J. B. Chung, S. K. Hansen, J. B. |
|---|---|
| author |
Chung, S. K. Hansen, J. B. |
| spellingShingle |
Chung, S. K. Hansen, J. B. Journal of Labelled Compounds and Radiopharmaceuticals Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions Organic Chemistry Spectroscopy Drug Discovery Radiology, Nuclear Medicine and imaging Biochemistry Analytical Chemistry |
| author_sort |
chung, s. k. |
| spelling |
Chung, S. K. Hansen, J. B. 0362-4803 1099-1344 Wiley Organic Chemistry Spectroscopy Drug Discovery Radiology, Nuclear Medicine and imaging Biochemistry Analytical Chemistry http://dx.doi.org/10.1002/jlcr.2580190119 <jats:title>Abstract</jats:title><jats:p>O,S‐Diethyl methylthiomalonate was efficiently condensed with paraformaldehyde‐<jats:sup>13</jats:sup>C in the presence of sodium methoxide to give 2‐[<jats:sup>13</jats:sup>C]‐hydroxymethylated product, which was converted to 2‐[<jats:sup>13</jats:sup>C]‐bromomethyl product by treatment with triphenylphosphine and carbon tetrabromide.</jats:p> Synthesis of O,S‐diethyl 2‐(bromomethyl‐<sup>13</sup>C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions Journal of Labelled Compounds and Radiopharmaceuticals |
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| title |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_unstemmed |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_full |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_fullStr |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_full_unstemmed |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_short |
Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_sort |
synthesis of o,s‐diethyl 2‐(bromomethyl‐<sup>13</sup>c)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| topic |
Organic Chemistry Spectroscopy Drug Discovery Radiology, Nuclear Medicine and imaging Biochemistry Analytical Chemistry |
| url |
http://dx.doi.org/10.1002/jlcr.2580190119 |
| publishDate |
1982 |
| physical |
151-153 |
| description |
<jats:title>Abstract</jats:title><jats:p>O,S‐Diethyl methylthiomalonate was efficiently condensed with paraformaldehyde‐<jats:sup>13</jats:sup>C in the presence of sodium methoxide to give 2‐[<jats:sup>13</jats:sup>C]‐hydroxymethylated product, which was converted to 2‐[<jats:sup>13</jats:sup>C]‐bromomethyl product by treatment with triphenylphosphine and carbon tetrabromide.</jats:p> |
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| description | <jats:title>Abstract</jats:title><jats:p>O,S‐Diethyl methylthiomalonate was efficiently condensed with paraformaldehyde‐<jats:sup>13</jats:sup>C in the presence of sodium methoxide to give 2‐[<jats:sup>13</jats:sup>C]‐hydroxymethylated product, which was converted to 2‐[<jats:sup>13</jats:sup>C]‐bromomethyl product by treatment with triphenylphosphine and carbon tetrabromide.</jats:p> |
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| imprint | Wiley, 1982 |
| imprint_str_mv | Wiley, 1982 |
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| physical | 151-153 |
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| series | Journal of Labelled Compounds and Radiopharmaceuticals |
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| spelling | Chung, S. K. Hansen, J. B. 0362-4803 1099-1344 Wiley Organic Chemistry Spectroscopy Drug Discovery Radiology, Nuclear Medicine and imaging Biochemistry Analytical Chemistry http://dx.doi.org/10.1002/jlcr.2580190119 <jats:title>Abstract</jats:title><jats:p>O,S‐Diethyl methylthiomalonate was efficiently condensed with paraformaldehyde‐<jats:sup>13</jats:sup>C in the presence of sodium methoxide to give 2‐[<jats:sup>13</jats:sup>C]‐hydroxymethylated product, which was converted to 2‐[<jats:sup>13</jats:sup>C]‐bromomethyl product by treatment with triphenylphosphine and carbon tetrabromide.</jats:p> Synthesis of O,S‐diethyl 2‐(bromomethyl‐<sup>13</sup>C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions Journal of Labelled Compounds and Radiopharmaceuticals |
| spellingShingle | Chung, S. K., Hansen, J. B., Journal of Labelled Compounds and Radiopharmaceuticals, Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions, Organic Chemistry, Spectroscopy, Drug Discovery, Radiology, Nuclear Medicine and imaging, Biochemistry, Analytical Chemistry |
| title | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_full | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_fullStr | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_full_unstemmed | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_short | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_sort | synthesis of o,s‐diethyl 2‐(bromomethyl‐<sup>13</sup>c)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| title_unstemmed | Synthesis of O,S‐diethyl 2‐(bromomethyl‐13C)‐2‐methylthiomalonate, a model substrate for methylmalonyl‐co a mutase reactions |
| topic | Organic Chemistry, Spectroscopy, Drug Discovery, Radiology, Nuclear Medicine and imaging, Biochemistry, Analytical Chemistry |
| url | http://dx.doi.org/10.1002/jlcr.2580190119 |