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A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water
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| Zeitschriftentitel: | Journal of Heterocyclic Chemistry |
|---|---|
| Personen und Körperschaften: | , |
| In: | Journal of Heterocyclic Chemistry, 53, 2016, 1, S. 32-37 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Wiley
|
| Schlagwörter: |
| author_facet |
Miklós, Ferenc Fülöp, Ferenc Miklós, Ferenc Fülöp, Ferenc |
|---|---|
| author |
Miklós, Ferenc Fülöp, Ferenc |
| spellingShingle |
Miklós, Ferenc Fülöp, Ferenc Journal of Heterocyclic Chemistry A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water Organic Chemistry |
| author_sort |
miklós, ferenc |
| spelling |
Miklós, Ferenc Fülöp, Ferenc 0022-152X 1943-5193 Wiley Organic Chemistry http://dx.doi.org/10.1002/jhet.1844 <jats:p>An environmentally benign condensation of anthranilic hydrazide with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one in aqueous medium has been developed for the synthesis of benzoylhydrazones A. The thermal rearrangements of hydrazones A yielded 3′‐aminospiro‐quinazolinones B. When A or B was reacted repeatedly with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one, spiroquinazoline‐hydrazones C were formed. From aqueous suspensions, products could be isolated in high purity by simple filtration.</jats:p> A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and <i>N</i>‐Benzylpiperidinone in Water Journal of Heterocyclic Chemistry |
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Wiley, 2016 |
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Journal of Heterocyclic Chemistry |
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| title |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_unstemmed |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_full |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_fullStr |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_full_unstemmed |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_short |
A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_sort |
a simple green protocol for the condensation of anthranilic hydrazide with cyclohexanone and <i>n</i>‐benzylpiperidinone in water |
| topic |
Organic Chemistry |
| url |
http://dx.doi.org/10.1002/jhet.1844 |
| publishDate |
2016 |
| physical |
32-37 |
| description |
<jats:p>An environmentally benign condensation of anthranilic hydrazide with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one in aqueous medium has been developed for the synthesis of benzoylhydrazones A. The thermal rearrangements of hydrazones A yielded 3′‐aminospiro‐quinazolinones B. When A or B was reacted repeatedly with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one, spiroquinazoline‐hydrazones C were formed. From aqueous suspensions, products could be isolated in high purity by simple filtration.</jats:p> |
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| author | Miklós, Ferenc, Fülöp, Ferenc |
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| description | <jats:p>An environmentally benign condensation of anthranilic hydrazide with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one in aqueous medium has been developed for the synthesis of benzoylhydrazones A. The thermal rearrangements of hydrazones A yielded 3′‐aminospiro‐quinazolinones B. When A or B was reacted repeatedly with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one, spiroquinazoline‐hydrazones C were formed. From aqueous suspensions, products could be isolated in high purity by simple filtration.</jats:p> |
| doi_str_mv | 10.1002/jhet.1844 |
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| imprint | Wiley, 2016 |
| imprint_str_mv | Wiley, 2016 |
| institution | DE-D275, DE-Bn3, DE-Brt1, DE-D161, DE-Gla1, DE-Zi4, DE-15, DE-Pl11, DE-Rs1, DE-105, DE-14, DE-Ch1, DE-L229 |
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| physical | 32-37 |
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| publishDateSort | 2016 |
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| series | Journal of Heterocyclic Chemistry |
| source_id | 49 |
| spelling | Miklós, Ferenc Fülöp, Ferenc 0022-152X 1943-5193 Wiley Organic Chemistry http://dx.doi.org/10.1002/jhet.1844 <jats:p>An environmentally benign condensation of anthranilic hydrazide with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one in aqueous medium has been developed for the synthesis of benzoylhydrazones A. The thermal rearrangements of hydrazones A yielded 3′‐aminospiro‐quinazolinones B. When A or B was reacted repeatedly with cyclohexanone or <jats:italic>N</jats:italic>‐benzylpiperidin‐4‐one, spiroquinazoline‐hydrazones C were formed. From aqueous suspensions, products could be isolated in high purity by simple filtration.</jats:p> A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and <i>N</i>‐Benzylpiperidinone in Water Journal of Heterocyclic Chemistry |
| spellingShingle | Miklós, Ferenc, Fülöp, Ferenc, Journal of Heterocyclic Chemistry, A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water, Organic Chemistry |
| title | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_full | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_fullStr | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_full_unstemmed | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_short | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| title_sort | a simple green protocol for the condensation of anthranilic hydrazide with cyclohexanone and <i>n</i>‐benzylpiperidinone in water |
| title_unstemmed | A Simple Green Protocol for the Condensation of Anthranilic Hydrazide with Cyclohexanone and N‐Benzylpiperidinone in Water |
| topic | Organic Chemistry |
| url | http://dx.doi.org/10.1002/jhet.1844 |