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Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane
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| Zeitschriftentitel: | Journal of Applied Polymer Science |
|---|---|
| Personen und Körperschaften: | , , , |
| In: | Journal of Applied Polymer Science, 82, 2001, 4, S. 929-933 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Wiley
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| Schlagwörter: |
| author_facet |
Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. |
|---|---|
| author |
Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. |
| spellingShingle |
Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. Journal of Applied Polymer Science Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane Materials Chemistry Polymers and Plastics Surfaces, Coatings and Films General Chemistry |
| author_sort |
zhou, n. |
| spelling |
Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. 0021-8995 1097-4628 Wiley Materials Chemistry Polymers and Plastics Surfaces, Coatings and Films General Chemistry http://dx.doi.org/10.1002/app.1924 <jats:title>Abstract</jats:title><jats:p>A new kind of polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was prepared by the anionic polymerization with a “seed solution” as initiator. The synthesis of monomers <jats:italic>N,N</jats:italic>′‐bis(hydroxydiphenylsilyl)tetraphenylcyclodisilazane (BHPTPC), <jats:italic>N,N</jats:italic>′‐bis(chlorodiphenylsilyl)tetraphenylcyclodisilazane (BCPTPC), and 1,3‐dichloro‐1,1,3,3‐tetraphenyldisilazane (DCTPS) are all reported in this study. The synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was characterized by <jats:sup>1</jats:sup>H–NMR, <jats:sup>29</jats:sup>Si–NMR, gel permeation chromatography (GPC), and intrinsic viscosity. The thermal stability of the polysiloxane was studied by isothermal gravimetric analysis (IGA). The results demonstrated that the synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane had excellent thermal stability. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 929–933, 2001</jats:p> Synthesis and properties of polysiloxane containing <i>N,N</i>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane Journal of Applied Polymer Science |
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| title |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_unstemmed |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_full |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_fullStr |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_full_unstemmed |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_short |
Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_sort |
synthesis and properties of polysiloxane containing <i>n,n</i>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| topic |
Materials Chemistry Polymers and Plastics Surfaces, Coatings and Films General Chemistry |
| url |
http://dx.doi.org/10.1002/app.1924 |
| publishDate |
2001 |
| physical |
929-933 |
| description |
<jats:title>Abstract</jats:title><jats:p>A new kind of polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was prepared by the anionic polymerization with a “seed solution” as initiator. The synthesis of monomers <jats:italic>N,N</jats:italic>′‐bis(hydroxydiphenylsilyl)tetraphenylcyclodisilazane (BHPTPC), <jats:italic>N,N</jats:italic>′‐bis(chlorodiphenylsilyl)tetraphenylcyclodisilazane (BCPTPC), and 1,3‐dichloro‐1,1,3,3‐tetraphenyldisilazane (DCTPS) are all reported in this study. The synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was characterized by <jats:sup>1</jats:sup>H–NMR, <jats:sup>29</jats:sup>Si–NMR, gel permeation chromatography (GPC), and intrinsic viscosity. The thermal stability of the polysiloxane was studied by isothermal gravimetric analysis (IGA). The results demonstrated that the synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane had excellent thermal stability. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 929–933, 2001</jats:p> |
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| author | Zhou, N., Zhang, Z. J., Xu, C. H., Xie, Z. M. |
| author_facet | Zhou, N., Zhang, Z. J., Xu, C. H., Xie, Z. M., Zhou, N., Zhang, Z. J., Xu, C. H., Xie, Z. M. |
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| description | <jats:title>Abstract</jats:title><jats:p>A new kind of polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was prepared by the anionic polymerization with a “seed solution” as initiator. The synthesis of monomers <jats:italic>N,N</jats:italic>′‐bis(hydroxydiphenylsilyl)tetraphenylcyclodisilazane (BHPTPC), <jats:italic>N,N</jats:italic>′‐bis(chlorodiphenylsilyl)tetraphenylcyclodisilazane (BCPTPC), and 1,3‐dichloro‐1,1,3,3‐tetraphenyldisilazane (DCTPS) are all reported in this study. The synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was characterized by <jats:sup>1</jats:sup>H–NMR, <jats:sup>29</jats:sup>Si–NMR, gel permeation chromatography (GPC), and intrinsic viscosity. The thermal stability of the polysiloxane was studied by isothermal gravimetric analysis (IGA). The results demonstrated that the synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane had excellent thermal stability. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 929–933, 2001</jats:p> |
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| spelling | Zhou, N. Zhang, Z. J. Xu, C. H. Xie, Z. M. 0021-8995 1097-4628 Wiley Materials Chemistry Polymers and Plastics Surfaces, Coatings and Films General Chemistry http://dx.doi.org/10.1002/app.1924 <jats:title>Abstract</jats:title><jats:p>A new kind of polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was prepared by the anionic polymerization with a “seed solution” as initiator. The synthesis of monomers <jats:italic>N,N</jats:italic>′‐bis(hydroxydiphenylsilyl)tetraphenylcyclodisilazane (BHPTPC), <jats:italic>N,N</jats:italic>′‐bis(chlorodiphenylsilyl)tetraphenylcyclodisilazane (BCPTPC), and 1,3‐dichloro‐1,1,3,3‐tetraphenyldisilazane (DCTPS) are all reported in this study. The synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane was characterized by <jats:sup>1</jats:sup>H–NMR, <jats:sup>29</jats:sup>Si–NMR, gel permeation chromatography (GPC), and intrinsic viscosity. The thermal stability of the polysiloxane was studied by isothermal gravimetric analysis (IGA). The results demonstrated that the synthesized polysiloxane containing <jats:italic>N,N</jats:italic>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane had excellent thermal stability. © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 929–933, 2001</jats:p> Synthesis and properties of polysiloxane containing <i>N,N</i>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane Journal of Applied Polymer Science |
| spellingShingle | Zhou, N., Zhang, Z. J., Xu, C. H., Xie, Z. M., Journal of Applied Polymer Science, Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane, Materials Chemistry, Polymers and Plastics, Surfaces, Coatings and Films, General Chemistry |
| title | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_full | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_fullStr | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_full_unstemmed | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_short | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_sort | synthesis and properties of polysiloxane containing <i>n,n</i>′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| title_unstemmed | Synthesis and properties of polysiloxane containing N,N′‐bis(diphenylsilyl)tetraphenylcyclodisilazane |
| topic | Materials Chemistry, Polymers and Plastics, Surfaces, Coatings and Films, General Chemistry |
| url | http://dx.doi.org/10.1002/app.1924 |