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A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile
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| Zeitschriftentitel: | Journal of AOAC INTERNATIONAL |
|---|---|
| Personen und Körperschaften: | , , , , , , , , |
| In: | Journal of AOAC INTERNATIONAL, 103, 2020, 4, S. 1181-1189 |
| Format: | E-Article |
| Sprache: | Englisch |
| veröffentlicht: |
Oxford University Press (OUP)
|
| Schlagwörter: |
| author_facet |
Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming |
|---|---|
| author |
Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming |
| spellingShingle |
Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming Journal of AOAC INTERNATIONAL A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry |
| author_sort |
duan, xiaoyun |
| spelling |
Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming 1060-3271 1944-7922 Oxford University Press (OUP) Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry http://dx.doi.org/10.1093/jaoacint/qsaa006 <jats:title>Abstract</jats:title> <jats:sec> <jats:title>Background</jats:title> <jats:p>Sulfonamides have been widely used in the prevention and clinical treatment of bacterial diseases in livestock and poultry. The use of sulfonamides increases the risk of veterinary drug residues in animal derived foods. The traditional reversed phase liquid chromatography methods for sulfonamides residues detection in animal derived foods have the problem of high consumption of organic solvents.</jats:p> </jats:sec> <jats:sec> <jats:title>Objective</jats:title> <jats:p>The aim of this study was to establish a green high-performance liquid chromatography method for the detection of sulfonamides residues in different animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Method</jats:title> <jats:p>The sample extraction solutions were purified by the Agela Cleanert PEP-2 cartridge and analyzed by the high-performance liquid chromatography method using ethanol as the green alternative solvent.</jats:p> </jats:sec> <jats:sec> <jats:title>Results</jats:title> <jats:p>The proposed method was validated in terms of linear range (20–1000 μg/kg), limit of detection (3.0–12.3 μg/kg), limit of quantitation (10–43 μg/kg), accuracy (80.7–101.3%), and repeatability and reproducibility (RSD &lt;5.9% and RSD &lt;8.5% respectively).</jats:p> </jats:sec> <jats:sec> <jats:title>Conclusions</jats:title> <jats:p>The proposed method is an environmentally friendly, sensitive and reliable high-performance liquid chromatography method for simultaneous determination of sulfonamide residues in animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Highlights</jats:title> <jats:p>In this work, we firstly developed a green high-performance liquid chromatography method for simultaneous determination of the residues of nine sulfonamides in milk and beef with ethanol as the green alternative solvent.</jats:p> </jats:sec> A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile Journal of AOAC INTERNATIONAL |
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10.1093/jaoacint/qsaa006 |
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Chemie und Pharmazie Land- und Forstwirtschaft, Gartenbau, Fischereiwirtschaft, Hauswirtschaft Technik |
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Oxford University Press (OUP), 2020 |
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1060-3271 1944-7922 |
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Journal of AOAC INTERNATIONAL |
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| title |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_unstemmed |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_full |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_fullStr |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_full_unstemmed |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_short |
A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_sort |
a green hplc method for determination of nine sulfonamides in milk and beef, and its greenness assessment with analytical eco-scale and greenness profile |
| topic |
Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry |
| url |
http://dx.doi.org/10.1093/jaoacint/qsaa006 |
| publishDate |
2020 |
| physical |
1181-1189 |
| description |
<jats:title>Abstract</jats:title>
<jats:sec>
<jats:title>Background</jats:title>
<jats:p>Sulfonamides have been widely used in the prevention and clinical treatment of bacterial diseases in livestock and poultry. The use of sulfonamides increases the risk of veterinary drug residues in animal derived foods. The traditional reversed phase liquid chromatography methods for sulfonamides residues detection in animal derived foods have the problem of high consumption of organic solvents.</jats:p>
</jats:sec>
<jats:sec>
<jats:title>Objective</jats:title>
<jats:p>The aim of this study was to establish a green high-performance liquid chromatography method for the detection of sulfonamides residues in different animal-origin foods.</jats:p>
</jats:sec>
<jats:sec>
<jats:title>Method</jats:title>
<jats:p>The sample extraction solutions were purified by the Agela Cleanert PEP-2 cartridge and analyzed by the high-performance liquid chromatography method using ethanol as the green alternative solvent.</jats:p>
</jats:sec>
<jats:sec>
<jats:title>Results</jats:title>
<jats:p>The proposed method was validated in terms of linear range (20–1000 μg/kg), limit of detection (3.0–12.3 μg/kg), limit of quantitation (10–43 μg/kg), accuracy (80.7–101.3%), and repeatability and reproducibility (RSD &lt;5.9% and RSD &lt;8.5% respectively).</jats:p>
</jats:sec>
<jats:sec>
<jats:title>Conclusions</jats:title>
<jats:p>The proposed method is an environmentally friendly, sensitive and reliable high-performance liquid chromatography method for simultaneous determination of sulfonamide residues in animal-origin foods.</jats:p>
</jats:sec>
<jats:sec>
<jats:title>Highlights</jats:title>
<jats:p>In this work, we firstly developed a green high-performance liquid chromatography method for simultaneous determination of the residues of nine sulfonamides in milk and beef with ethanol as the green alternative solvent.</jats:p>
</jats:sec> |
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| author | Duan, Xiaoyun, Liu, Xiaofeng, Dong, Yue, Yang, Jing, Zhang, Jing, He, Shujuan, Yang, Fatang, Wang, Zhen, Dong, Yuming |
| author_facet | Duan, Xiaoyun, Liu, Xiaofeng, Dong, Yue, Yang, Jing, Zhang, Jing, He, Shujuan, Yang, Fatang, Wang, Zhen, Dong, Yuming, Duan, Xiaoyun, Liu, Xiaofeng, Dong, Yue, Yang, Jing, Zhang, Jing, He, Shujuan, Yang, Fatang, Wang, Zhen, Dong, Yuming |
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| description | <jats:title>Abstract</jats:title> <jats:sec> <jats:title>Background</jats:title> <jats:p>Sulfonamides have been widely used in the prevention and clinical treatment of bacterial diseases in livestock and poultry. The use of sulfonamides increases the risk of veterinary drug residues in animal derived foods. The traditional reversed phase liquid chromatography methods for sulfonamides residues detection in animal derived foods have the problem of high consumption of organic solvents.</jats:p> </jats:sec> <jats:sec> <jats:title>Objective</jats:title> <jats:p>The aim of this study was to establish a green high-performance liquid chromatography method for the detection of sulfonamides residues in different animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Method</jats:title> <jats:p>The sample extraction solutions were purified by the Agela Cleanert PEP-2 cartridge and analyzed by the high-performance liquid chromatography method using ethanol as the green alternative solvent.</jats:p> </jats:sec> <jats:sec> <jats:title>Results</jats:title> <jats:p>The proposed method was validated in terms of linear range (20–1000 μg/kg), limit of detection (3.0–12.3 μg/kg), limit of quantitation (10–43 μg/kg), accuracy (80.7–101.3%), and repeatability and reproducibility (RSD &lt;5.9% and RSD &lt;8.5% respectively).</jats:p> </jats:sec> <jats:sec> <jats:title>Conclusions</jats:title> <jats:p>The proposed method is an environmentally friendly, sensitive and reliable high-performance liquid chromatography method for simultaneous determination of sulfonamide residues in animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Highlights</jats:title> <jats:p>In this work, we firstly developed a green high-performance liquid chromatography method for simultaneous determination of the residues of nine sulfonamides in milk and beef with ethanol as the green alternative solvent.</jats:p> </jats:sec> |
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| imprint | Oxford University Press (OUP), 2020 |
| imprint_str_mv | Oxford University Press (OUP), 2020 |
| institution | DE-Gla1, DE-Zi4, DE-15, DE-Pl11, DE-Rs1, DE-14, DE-Ch1, DE-L229, DE-D275, DE-Bn3, DE-Brt1, DE-D161 |
| issn | 1060-3271, 1944-7922 |
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| physical | 1181-1189 |
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| spelling | Duan, Xiaoyun Liu, Xiaofeng Dong, Yue Yang, Jing Zhang, Jing He, Shujuan Yang, Fatang Wang, Zhen Dong, Yuming 1060-3271 1944-7922 Oxford University Press (OUP) Pharmacology Agronomy and Crop Science Environmental Chemistry Food Science Analytical Chemistry http://dx.doi.org/10.1093/jaoacint/qsaa006 <jats:title>Abstract</jats:title> <jats:sec> <jats:title>Background</jats:title> <jats:p>Sulfonamides have been widely used in the prevention and clinical treatment of bacterial diseases in livestock and poultry. The use of sulfonamides increases the risk of veterinary drug residues in animal derived foods. The traditional reversed phase liquid chromatography methods for sulfonamides residues detection in animal derived foods have the problem of high consumption of organic solvents.</jats:p> </jats:sec> <jats:sec> <jats:title>Objective</jats:title> <jats:p>The aim of this study was to establish a green high-performance liquid chromatography method for the detection of sulfonamides residues in different animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Method</jats:title> <jats:p>The sample extraction solutions were purified by the Agela Cleanert PEP-2 cartridge and analyzed by the high-performance liquid chromatography method using ethanol as the green alternative solvent.</jats:p> </jats:sec> <jats:sec> <jats:title>Results</jats:title> <jats:p>The proposed method was validated in terms of linear range (20–1000 μg/kg), limit of detection (3.0–12.3 μg/kg), limit of quantitation (10–43 μg/kg), accuracy (80.7–101.3%), and repeatability and reproducibility (RSD &lt;5.9% and RSD &lt;8.5% respectively).</jats:p> </jats:sec> <jats:sec> <jats:title>Conclusions</jats:title> <jats:p>The proposed method is an environmentally friendly, sensitive and reliable high-performance liquid chromatography method for simultaneous determination of sulfonamide residues in animal-origin foods.</jats:p> </jats:sec> <jats:sec> <jats:title>Highlights</jats:title> <jats:p>In this work, we firstly developed a green high-performance liquid chromatography method for simultaneous determination of the residues of nine sulfonamides in milk and beef with ethanol as the green alternative solvent.</jats:p> </jats:sec> A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile Journal of AOAC INTERNATIONAL |
| spellingShingle | Duan, Xiaoyun, Liu, Xiaofeng, Dong, Yue, Yang, Jing, Zhang, Jing, He, Shujuan, Yang, Fatang, Wang, Zhen, Dong, Yuming, Journal of AOAC INTERNATIONAL, A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile, Pharmacology, Agronomy and Crop Science, Environmental Chemistry, Food Science, Analytical Chemistry |
| title | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_full | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_fullStr | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_full_unstemmed | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_short | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| title_sort | a green hplc method for determination of nine sulfonamides in milk and beef, and its greenness assessment with analytical eco-scale and greenness profile |
| title_unstemmed | A Green HPLC Method for Determination of Nine Sulfonamides in Milk and Beef, and Its Greenness Assessment with Analytical Eco-Scale and Greenness Profile |
| topic | Pharmacology, Agronomy and Crop Science, Environmental Chemistry, Food Science, Analytical Chemistry |
| url | http://dx.doi.org/10.1093/jaoacint/qsaa006 |