author_facet Ford, J. E.
Hurrell, R. F.
Finot, P. A.
Ford, J. E.
Hurrell, R. F.
Finot, P. A.
author Ford, J. E.
Hurrell, R. F.
Finot, P. A.
spellingShingle Ford, J. E.
Hurrell, R. F.
Finot, P. A.
British Journal of Nutrition
Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
Nutrition and Dietetics
Medicine (miscellaneous)
author_sort ford, j. e.
spelling Ford, J. E. Hurrell, R. F. Finot, P. A. 0007-1145 1475-2662 Cambridge University Press (CUP) Nutrition and Dietetics Medicine (miscellaneous) http://dx.doi.org/10.1079/bjn19830044 <jats:p>1. Storage of milk powder under unfavourable conditions accelerates the normally slow deterioration in nutritional quality. The effects of such storage on the water-soluble vitamin composition were examined.</jats:p><jats:p>2. (<jats:italic>a</jats:italic>) Spray-dried whole milk containing 25 g water/kg was stored at 60° and 70° and sampled weekly to 9 weeks. (<jats:italic>b</jats:italic>) Spray-dried whole milk and skimmed milk were adjusted to contain 40 and 100 g water/kg and stored at 37° in nitrogenand in oxygen. Samples were taken for analysis at intervals during storage.</jats:p><jats:p>3. The samples were analysed for eight B-complex vitamins and ascorbic acid, and also for total lysine, ‘reactive lysine’ and ‘lysine as lactulosyl-lysine’.</jats:p><jats:p>4. Storage at 60° caused rapid destruction of folic acid (53% loss at 4 weeks) and slower loss of thiamin, vitamin B<jats:sub>6</jats:sub> and pantothenic acid (18% at 8 weeks). There was no change in the content of riboflavin, biotin, nicotinic acid and vitamin B<jats:sub>12</jats:sub>. At 70° the rate of destruction of the four labile vitamins was much increased; 18% or less survived at 4 weeks.</jats:p><jats:p>5. At 37° and 40 g water/kg there was little change in total and ‘reactive’ lysine during storage for 57 d. Lactulosyl-lysine was demonstrably present butatlow concentration. There was considerable loss of folate (72%) and ascorbate (91%) during storage for 30 d in O<jats:sub>2</jats:sub>, but no significant loss in N<jats:sub>2</jats:sub>. Thiamin fell by approximately 12% in 57 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. The content of the remaining vitamins was unchanged. At 100 g water/kg there were progressive Maillard changes. During 27 d in N<jats:sub>2</jats:sub> the colour changed from cream to palebrown, but in O<jats:sub>2</jats:sub> there was no perceptible colour change. Total lysine fell by 20% in 27 d, and ‘reactive lysine’ by 30%. Folate was stable during 16 d in N<jats:sub>2</jats:sub>, but largely (94%) destroyed in O<jats:sub>2</jats:sub>. Ascorbic acid was also destroyed in N<jats:sub>2</jats:sub> as in O<jats:sub>2</jats:sub>. Thiamin fell by 41% in 27 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. Vitamin B<jats:sub>6</jats:sub> was more labile, especially in N<jats:sub>2</jats:sub>, falling by 71% in 16d.</jats:p><jats:p>6. With skimmed-milk powder containing 100 g water/kg, storage at 37° in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub> gave much the same results as for the corresponding whole-milk powder. The presence of milk fat had no marked effect on the stability of the water-soluble vitamins.</jats:p><jats:p>7. Destruction of vitamins was clearly linked to the progress of Maillard-type reactions and was strongly influenced by time and temperature of storage, moisture content and, in some instances, by the presence of O<jats:sub>2</jats:sub>.</jats:p> 2. Influence on the content of water-soluble vitamins Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins British Journal of Nutrition
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series British Journal of Nutrition
source_id 49
title_sub 2. Influence on the content of water-soluble vitamins
title Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_unstemmed Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_full Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_fullStr Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_full_unstemmed Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_short Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_sort storage of milk powders under adverse conditions : 2. influence on the content of water-soluble vitamins
topic Nutrition and Dietetics
Medicine (miscellaneous)
url http://dx.doi.org/10.1079/bjn19830044
publishDate 1983
physical 355-364
description <jats:p>1. Storage of milk powder under unfavourable conditions accelerates the normally slow deterioration in nutritional quality. The effects of such storage on the water-soluble vitamin composition were examined.</jats:p><jats:p>2. (<jats:italic>a</jats:italic>) Spray-dried whole milk containing 25 g water/kg was stored at 60° and 70° and sampled weekly to 9 weeks. (<jats:italic>b</jats:italic>) Spray-dried whole milk and skimmed milk were adjusted to contain 40 and 100 g water/kg and stored at 37° in nitrogenand in oxygen. Samples were taken for analysis at intervals during storage.</jats:p><jats:p>3. The samples were analysed for eight B-complex vitamins and ascorbic acid, and also for total lysine, ‘reactive lysine’ and ‘lysine as lactulosyl-lysine’.</jats:p><jats:p>4. Storage at 60° caused rapid destruction of folic acid (53% loss at 4 weeks) and slower loss of thiamin, vitamin B<jats:sub>6</jats:sub> and pantothenic acid (18% at 8 weeks). There was no change in the content of riboflavin, biotin, nicotinic acid and vitamin B<jats:sub>12</jats:sub>. At 70° the rate of destruction of the four labile vitamins was much increased; 18% or less survived at 4 weeks.</jats:p><jats:p>5. At 37° and 40 g water/kg there was little change in total and ‘reactive’ lysine during storage for 57 d. Lactulosyl-lysine was demonstrably present butatlow concentration. There was considerable loss of folate (72%) and ascorbate (91%) during storage for 30 d in O<jats:sub>2</jats:sub>, but no significant loss in N<jats:sub>2</jats:sub>. Thiamin fell by approximately 12% in 57 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. The content of the remaining vitamins was unchanged. At 100 g water/kg there were progressive Maillard changes. During 27 d in N<jats:sub>2</jats:sub> the colour changed from cream to palebrown, but in O<jats:sub>2</jats:sub> there was no perceptible colour change. Total lysine fell by 20% in 27 d, and ‘reactive lysine’ by 30%. Folate was stable during 16 d in N<jats:sub>2</jats:sub>, but largely (94%) destroyed in O<jats:sub>2</jats:sub>. Ascorbic acid was also destroyed in N<jats:sub>2</jats:sub> as in O<jats:sub>2</jats:sub>. Thiamin fell by 41% in 27 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. Vitamin B<jats:sub>6</jats:sub> was more labile, especially in N<jats:sub>2</jats:sub>, falling by 71% in 16d.</jats:p><jats:p>6. With skimmed-milk powder containing 100 g water/kg, storage at 37° in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub> gave much the same results as for the corresponding whole-milk powder. The presence of milk fat had no marked effect on the stability of the water-soluble vitamins.</jats:p><jats:p>7. Destruction of vitamins was clearly linked to the progress of Maillard-type reactions and was strongly influenced by time and temperature of storage, moisture content and, in some instances, by the presence of O<jats:sub>2</jats:sub>.</jats:p>
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author Ford, J. E., Hurrell, R. F., Finot, P. A.
author_facet Ford, J. E., Hurrell, R. F., Finot, P. A., Ford, J. E., Hurrell, R. F., Finot, P. A.
author_sort ford, j. e.
container_issue 3
container_start_page 355
container_title British Journal of Nutrition
container_volume 49
description <jats:p>1. Storage of milk powder under unfavourable conditions accelerates the normally slow deterioration in nutritional quality. The effects of such storage on the water-soluble vitamin composition were examined.</jats:p><jats:p>2. (<jats:italic>a</jats:italic>) Spray-dried whole milk containing 25 g water/kg was stored at 60° and 70° and sampled weekly to 9 weeks. (<jats:italic>b</jats:italic>) Spray-dried whole milk and skimmed milk were adjusted to contain 40 and 100 g water/kg and stored at 37° in nitrogenand in oxygen. Samples were taken for analysis at intervals during storage.</jats:p><jats:p>3. The samples were analysed for eight B-complex vitamins and ascorbic acid, and also for total lysine, ‘reactive lysine’ and ‘lysine as lactulosyl-lysine’.</jats:p><jats:p>4. Storage at 60° caused rapid destruction of folic acid (53% loss at 4 weeks) and slower loss of thiamin, vitamin B<jats:sub>6</jats:sub> and pantothenic acid (18% at 8 weeks). There was no change in the content of riboflavin, biotin, nicotinic acid and vitamin B<jats:sub>12</jats:sub>. At 70° the rate of destruction of the four labile vitamins was much increased; 18% or less survived at 4 weeks.</jats:p><jats:p>5. At 37° and 40 g water/kg there was little change in total and ‘reactive’ lysine during storage for 57 d. Lactulosyl-lysine was demonstrably present butatlow concentration. There was considerable loss of folate (72%) and ascorbate (91%) during storage for 30 d in O<jats:sub>2</jats:sub>, but no significant loss in N<jats:sub>2</jats:sub>. Thiamin fell by approximately 12% in 57 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. The content of the remaining vitamins was unchanged. At 100 g water/kg there were progressive Maillard changes. During 27 d in N<jats:sub>2</jats:sub> the colour changed from cream to palebrown, but in O<jats:sub>2</jats:sub> there was no perceptible colour change. Total lysine fell by 20% in 27 d, and ‘reactive lysine’ by 30%. Folate was stable during 16 d in N<jats:sub>2</jats:sub>, but largely (94%) destroyed in O<jats:sub>2</jats:sub>. Ascorbic acid was also destroyed in N<jats:sub>2</jats:sub> as in O<jats:sub>2</jats:sub>. Thiamin fell by 41% in 27 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. Vitamin B<jats:sub>6</jats:sub> was more labile, especially in N<jats:sub>2</jats:sub>, falling by 71% in 16d.</jats:p><jats:p>6. With skimmed-milk powder containing 100 g water/kg, storage at 37° in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub> gave much the same results as for the corresponding whole-milk powder. The presence of milk fat had no marked effect on the stability of the water-soluble vitamins.</jats:p><jats:p>7. Destruction of vitamins was clearly linked to the progress of Maillard-type reactions and was strongly influenced by time and temperature of storage, moisture content and, in some instances, by the presence of O<jats:sub>2</jats:sub>.</jats:p>
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spelling Ford, J. E. Hurrell, R. F. Finot, P. A. 0007-1145 1475-2662 Cambridge University Press (CUP) Nutrition and Dietetics Medicine (miscellaneous) http://dx.doi.org/10.1079/bjn19830044 <jats:p>1. Storage of milk powder under unfavourable conditions accelerates the normally slow deterioration in nutritional quality. The effects of such storage on the water-soluble vitamin composition were examined.</jats:p><jats:p>2. (<jats:italic>a</jats:italic>) Spray-dried whole milk containing 25 g water/kg was stored at 60° and 70° and sampled weekly to 9 weeks. (<jats:italic>b</jats:italic>) Spray-dried whole milk and skimmed milk were adjusted to contain 40 and 100 g water/kg and stored at 37° in nitrogenand in oxygen. Samples were taken for analysis at intervals during storage.</jats:p><jats:p>3. The samples were analysed for eight B-complex vitamins and ascorbic acid, and also for total lysine, ‘reactive lysine’ and ‘lysine as lactulosyl-lysine’.</jats:p><jats:p>4. Storage at 60° caused rapid destruction of folic acid (53% loss at 4 weeks) and slower loss of thiamin, vitamin B<jats:sub>6</jats:sub> and pantothenic acid (18% at 8 weeks). There was no change in the content of riboflavin, biotin, nicotinic acid and vitamin B<jats:sub>12</jats:sub>. At 70° the rate of destruction of the four labile vitamins was much increased; 18% or less survived at 4 weeks.</jats:p><jats:p>5. At 37° and 40 g water/kg there was little change in total and ‘reactive’ lysine during storage for 57 d. Lactulosyl-lysine was demonstrably present butatlow concentration. There was considerable loss of folate (72%) and ascorbate (91%) during storage for 30 d in O<jats:sub>2</jats:sub>, but no significant loss in N<jats:sub>2</jats:sub>. Thiamin fell by approximately 12% in 57 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. The content of the remaining vitamins was unchanged. At 100 g water/kg there were progressive Maillard changes. During 27 d in N<jats:sub>2</jats:sub> the colour changed from cream to palebrown, but in O<jats:sub>2</jats:sub> there was no perceptible colour change. Total lysine fell by 20% in 27 d, and ‘reactive lysine’ by 30%. Folate was stable during 16 d in N<jats:sub>2</jats:sub>, but largely (94%) destroyed in O<jats:sub>2</jats:sub>. Ascorbic acid was also destroyed in N<jats:sub>2</jats:sub> as in O<jats:sub>2</jats:sub>. Thiamin fell by 41% in 27 d, equally in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub>. Vitamin B<jats:sub>6</jats:sub> was more labile, especially in N<jats:sub>2</jats:sub>, falling by 71% in 16d.</jats:p><jats:p>6. With skimmed-milk powder containing 100 g water/kg, storage at 37° in O<jats:sub>2</jats:sub> and N<jats:sub>2</jats:sub> gave much the same results as for the corresponding whole-milk powder. The presence of milk fat had no marked effect on the stability of the water-soluble vitamins.</jats:p><jats:p>7. Destruction of vitamins was clearly linked to the progress of Maillard-type reactions and was strongly influenced by time and temperature of storage, moisture content and, in some instances, by the presence of O<jats:sub>2</jats:sub>.</jats:p> 2. Influence on the content of water-soluble vitamins Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins British Journal of Nutrition
spellingShingle Ford, J. E., Hurrell, R. F., Finot, P. A., British Journal of Nutrition, Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins, Nutrition and Dietetics, Medicine (miscellaneous)
title Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_full Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_fullStr Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_full_unstemmed Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_short Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
title_sort storage of milk powders under adverse conditions : 2. influence on the content of water-soluble vitamins
title_sub 2. Influence on the content of water-soluble vitamins
title_unstemmed Storage of milk powders under adverse conditions : 2. Influence on the content of water-soluble vitamins
topic Nutrition and Dietetics, Medicine (miscellaneous)
url http://dx.doi.org/10.1079/bjn19830044