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Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes
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Zeitschriftentitel: | Rapid Communications in Mass Spectrometry |
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Personen und Körperschaften: | , , , , , |
In: | Rapid Communications in Mass Spectrometry, 25, 2011, 3, S. 436-442 |
Format: | E-Article |
Sprache: | Englisch |
veröffentlicht: |
Wiley
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Schlagwörter: |
author_facet |
Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. |
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author |
Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. |
spellingShingle |
Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. Rapid Communications in Mass Spectrometry Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes Organic Chemistry Spectroscopy Analytical Chemistry |
author_sort |
zhou, simon ningsun |
spelling |
Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. 0951-4198 1097-0231 Wiley Organic Chemistry Spectroscopy Analytical Chemistry http://dx.doi.org/10.1002/rcm.4874 <jats:title>Abstract</jats:title><jats:p>Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry (LC/APPI‐MS/MS) was investigated as an instrumental method for the analysis of the halogenated norbornene flame retardants, Mirex, Dechloranes 602, 603, 604, and Dechlorane Plus (DP). The LC separation was optimized by screening a variety of stationary and mobile phases, resulting in a short LC separation time of 5 min. Different atmospheric pressure ionization approaches were examined including electrospray ionization, atmospheric pressure chemical ionization, and APPI, each with and without post‐column addition. APPI without post‐column addition was chosen for providing the best ionization response. The optimized LC/APPI‐MS/MS approach resulted in instrument detection limits ranging between 25 and 50 pg. Good linearity was also achieved (up to 25.0 ng/µL; <jats:italic>R</jats:italic> >0.999). The method was applied to extracts of environmental samples including surface water, fish and sediments for screening purposes, and the results agreed well with those obtained by gas chromatography/mass spectrometry. Copyright © 2011 John Wiley & Sons, Ltd.</jats:p> Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes Rapid Communications in Mass Spectrometry |
doi_str_mv |
10.1002/rcm.4874 |
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2011 |
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Wiley |
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Rapid Communications in Mass Spectrometry |
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title |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_unstemmed |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_full |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_fullStr |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_full_unstemmed |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_short |
Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_sort |
liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of dechloranes |
topic |
Organic Chemistry Spectroscopy Analytical Chemistry |
url |
http://dx.doi.org/10.1002/rcm.4874 |
publishDate |
2011 |
physical |
436-442 |
description |
<jats:title>Abstract</jats:title><jats:p>Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry (LC/APPI‐MS/MS) was investigated as an instrumental method for the analysis of the halogenated norbornene flame retardants, Mirex, Dechloranes 602, 603, 604, and Dechlorane Plus (DP). The LC separation was optimized by screening a variety of stationary and mobile phases, resulting in a short LC separation time of 5 min. Different atmospheric pressure ionization approaches were examined including electrospray ionization, atmospheric pressure chemical ionization, and APPI, each with and without post‐column addition. APPI without post‐column addition was chosen for providing the best ionization response. The optimized LC/APPI‐MS/MS approach resulted in instrument detection limits ranging between 25 and 50 pg. Good linearity was also achieved (up to 25.0 ng/µL; <jats:italic>R</jats:italic> >0.999). The method was applied to extracts of environmental samples including surface water, fish and sediments for screening purposes, and the results agreed well with those obtained by gas chromatography/mass spectrometry. Copyright © 2011 John Wiley & Sons, Ltd.</jats:p> |
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author | Zhou, Simon Ningsun, Reiner, Eric J., Marvin, Chris H., Helm, Paul A., Shen, Li, Brindle, Ian D. |
author_facet | Zhou, Simon Ningsun, Reiner, Eric J., Marvin, Chris H., Helm, Paul A., Shen, Li, Brindle, Ian D., Zhou, Simon Ningsun, Reiner, Eric J., Marvin, Chris H., Helm, Paul A., Shen, Li, Brindle, Ian D. |
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container_title | Rapid Communications in Mass Spectrometry |
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description | <jats:title>Abstract</jats:title><jats:p>Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry (LC/APPI‐MS/MS) was investigated as an instrumental method for the analysis of the halogenated norbornene flame retardants, Mirex, Dechloranes 602, 603, 604, and Dechlorane Plus (DP). The LC separation was optimized by screening a variety of stationary and mobile phases, resulting in a short LC separation time of 5 min. Different atmospheric pressure ionization approaches were examined including electrospray ionization, atmospheric pressure chemical ionization, and APPI, each with and without post‐column addition. APPI without post‐column addition was chosen for providing the best ionization response. The optimized LC/APPI‐MS/MS approach resulted in instrument detection limits ranging between 25 and 50 pg. Good linearity was also achieved (up to 25.0 ng/µL; <jats:italic>R</jats:italic> >0.999). The method was applied to extracts of environmental samples including surface water, fish and sediments for screening purposes, and the results agreed well with those obtained by gas chromatography/mass spectrometry. Copyright © 2011 John Wiley & Sons, Ltd.</jats:p> |
doi_str_mv | 10.1002/rcm.4874 |
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spelling | Zhou, Simon Ningsun Reiner, Eric J. Marvin, Chris H. Helm, Paul A. Shen, Li Brindle, Ian D. 0951-4198 1097-0231 Wiley Organic Chemistry Spectroscopy Analytical Chemistry http://dx.doi.org/10.1002/rcm.4874 <jats:title>Abstract</jats:title><jats:p>Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry (LC/APPI‐MS/MS) was investigated as an instrumental method for the analysis of the halogenated norbornene flame retardants, Mirex, Dechloranes 602, 603, 604, and Dechlorane Plus (DP). The LC separation was optimized by screening a variety of stationary and mobile phases, resulting in a short LC separation time of 5 min. Different atmospheric pressure ionization approaches were examined including electrospray ionization, atmospheric pressure chemical ionization, and APPI, each with and without post‐column addition. APPI without post‐column addition was chosen for providing the best ionization response. The optimized LC/APPI‐MS/MS approach resulted in instrument detection limits ranging between 25 and 50 pg. Good linearity was also achieved (up to 25.0 ng/µL; <jats:italic>R</jats:italic> >0.999). The method was applied to extracts of environmental samples including surface water, fish and sediments for screening purposes, and the results agreed well with those obtained by gas chromatography/mass spectrometry. Copyright © 2011 John Wiley & Sons, Ltd.</jats:p> Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes Rapid Communications in Mass Spectrometry |
spellingShingle | Zhou, Simon Ningsun, Reiner, Eric J., Marvin, Chris H., Helm, Paul A., Shen, Li, Brindle, Ian D., Rapid Communications in Mass Spectrometry, Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes, Organic Chemistry, Spectroscopy, Analytical Chemistry |
title | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_full | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_fullStr | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_full_unstemmed | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_short | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
title_sort | liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of dechloranes |
title_unstemmed | Liquid chromatography/atmospheric pressure photoionization tandem mass spectrometry for analysis of Dechloranes |
topic | Organic Chemistry, Spectroscopy, Analytical Chemistry |
url | http://dx.doi.org/10.1002/rcm.4874 |